Citation: LONG Qin, ZHOU Dali, ZHANG Xiang, WEI Dong-Juan, LIU Shu-Jing, CHEN Dong-Lin. Preparation of a Silane Coupling Agent and Surface Modification of Apatite-Wollastonite Bioactive Glass-Ceramic[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(5): 948-952. doi: 10.3969/j.issn.1001-4861.2013.00.147 shu

Preparation of a Silane Coupling Agent and Surface Modification of Apatite-Wollastonite Bioactive Glass-Ceramic

1.
College of Materials Science and Engineering, Sichuan University, Chengdu 610064, China

Corresponding author: ZHOU Dali,
Received Date: 19 October 2012
Available Online: 7 January 2013
Fund Project: 四川大学2011年青年基金(No.2082604154120)资助项目。 (No.2082604154120)

In this work, a kind of silane coupling agent was prepared by condensation reaction of the glutamic acid and silane coupling agent (KH-792). The Glutamic acid was attached to the surface of Apatite-wollastonite bioactive glass-ceramic (A-W GC) by the bifunctional cross-linking agent. To evaluate in vitro cytocompatibility, the surface modified material was co-cultured with the 5th generation human osteosarcoma cell MG63. Fourier Transform infrared spectroscopy (FTIR), Scanning Electron Microscope (SEM), and X-ray Photoelectron Spectroscopy (XPS) were used to character the structure and performance of the synthetic coupling agent and the surface modified A-W GC, respectively. The results show that the Glutamic acid and KH-792 were connected by amide groups, and A-W GC is effectively modified by the synthetic coupling agent. The MG63 cell experiments show that cells adhered to the surface of the material, and the cell proliferation on the surface of the material was promoted. It is an effective method to improve the cell compatibility of A-W GC by surface modification.
- silane coupling agent;glutamic acid;apatite-wollastonite bioactive glass-ceramic;surface modification
1. [1]
  [1] Yang C L, Cheng K, Weng W J, et al. J. Mater. Sci.: Mater. Med., 2009,20(11):2349-2352
2. [2]
  [2] Mathews D T, Birney Y A, Cahill P A, et al. J. Biomed. Mater. Res. Part B: App. Biomate., 2008,84(2):531-540
3. [3]
  [3] Feng Y K, Guo J T. Int. J. Mol. Sci., 2009,10(2):589-61
4. [4]
  [4] Williams D F. Biomaterials, 2008,29(20):2941-2953
5. [5]
  [5] Silveira A C C, Lima R S, Penha E M, et al. Veterinary Immunol. Immunopathol., 2009,128(1-3):342
6. [6]
  [6] Feng Q, Chow P K, Frassoni F, et al. Exp. Hematol., 2008, 36(11):1556-1566
7. [7]
  [7] LI Guang-Da(李光大),ZHOU Da-Li(周大利), FENG Dan-Ge (冯丹歌), et al. J. Inorg. Mater. (Wuji Cailiao Xuebao), 2008, 23(3):621-625
8. [8]
  [8] XUE Ming(薛明), FENG Dan-Ge(冯丹歌), LI Guang-Da (李光大), et al. Chinese J. Inorg. Chem.(Wuji Huaxue Xuebao), 2007,23(4):708-712
9. [9]
  [9] YAO Hui-Mei(姚辉梅), SANG Tai-You(商太友), MENG Xiang(孟祥), et al. Guangzhou Chem. Ind. (Guangzhou Huagong), 2011,39(22):61-62
10. [10]
  [10] LIAO Jian-Guo(廖建国), WANG Xue-Jiang(王学江), ZUO Yi(左奕), et al. J. Inorg. Mater.(Wuji Cailiao Xuebao), 2008, 23(1):145-149
11. [11]
  [11] Shelton R M, Rasmussen A C, Davies J E. Biomaterials, 1988,9(1):24-29
12. [12]
  [12] Massia S P, Hubbell J A. J. Biol. Chem., 1992,267(14): 10133-10141
13. [13]
  [13] Tamada Y, Ikada Y. J. Biomed. Mater. Res., 1994,28(7): 783-789
14. [14]
  [14] Lee J H, Jung H W, Kang I K, et al. Biomaterials, 1994,15 (9):705-711
15. [15]
  [15] Cook A D, Hrkach J S, Gao N N, et al. J. Biomed. Mater. Res., 1997,35(4):513-523
16. [16]
  [16] FENG Dan-Ge(冯丹歌), ZHOU Da-Li(周大利), LONG Qin (龙沁), et al. Chin. J. Tissue Engi. Res. (Zhongguo Zuzhi Gongcheng Yanjiu Yu Linchuang Kangfu), 2009,13(12): 2253-2256
17. [17]
  [17] LIU Gang(刘刚). Thesis for the Doctorate of the Fourth Military Medical University(第四军医大学博士论文). 2003.
18. [18]
  [18] LUO Chun-Hua(罗春华), DONG Qiu-Jing(董秋静), CAO Jian(曹健),et al. J. Fuyang Teachers College: Nat. Sci. (Fuyang Shifan Xueyuan Xuebao: Ziran Kexue Ban), 2010, 27(1):1-4
19. [19]
  [19] WANG Wei-Chen(王伟宸),LIU Wei(刘伟). J. Beijing Univ. Chem. Technol.: Nat. Sci.(Beijing Huagong Daxue Xuebao: Ziran Kexue Ban), 2010,37(2):16-20
20. [20]
  [20] LI Mu-Qin(李慕勤), GUAN Da-Wei(管大为), WANG Jing- Yan(王晶彦), et al. J. Ceram.(Taoci Xuebao), 2008,29(4): 344-347
21. [21]
  [21] LI Xian-Xue(李先学),SHEN Gao-Yang(沈高扬), YANG Lei (杨磊), et al. Chin. J. Rare Metals(Zhongguo Xitu Xuebao), 2011,35(4):613-616
22. [22]
  [22] JI Xiao-Li(吉晓莉), ZHENG Cai-Hua(郑彩华), WEI Lei (魏磊), et al. Chem. Bioengin.(Huaxue Yu Shengwu Gongcheng), 2008,25(1):21-23
1. [1]
  Shijie Ren , Mingze Gao , Rui-Ting Gao , Lei Wang . Bimetallic Oxyhydroxide Cocatalyst Derived from CoFe MOF for Stable Solar Water Splitting. Acta Physico-Chimica Sinica, 2024, 40(7): 2307040-0. doi: 10.3866/PKU.WHXB202307040
2. [2]
  Hanmei Lü , Xin Chen , Qifu Sun , Ning Zhao , Xiangxin Guo . Uniform Garnet Nanoparticle Dispersion in Composite Polymer Electrolytes. Acta Physico-Chimica Sinica, 2024, 40(3): 2305016-0. doi: 10.3866/PKU.WHXB202305016
3. [3]
  Jie WU , Zhihong LUO , Xiaoli CHEN , Fangfang XIONG , Li CHEN , Biao ZHANG , Bin SHI , Quansheng OUYANG , Jiaojing SHAO . Critical roles of AlPO₄ coating in enhancing cycling stability and rate capability of high voltage LiNi_0.5Mn_1.5O₄ cathode materials. Chinese Journal of Inorganic Chemistry, 2025, 41(5): 948-958. doi: 10.11862/CJIC.20240400
4. [4]
  Junjian Wang , Qingquan Yu , Shunyao Liu , Yuke Chen , Xiaoyu Liu , Guodong Li , Xiaoyan Liu , Hong Liu , Weijia Zhou . Laser-Induced Carbonization of Hydroxyapatite Sandwich Paper for Inkless Printing. Acta Physico-Chimica Sinica, 2024, 40(4): 2304024-0. doi: 10.3866/PKU.WHXB202304024
5. [5]
  Hailian Tang , Siyuan Chen , Qiaoyun Liu , Guoyi Bai , Botao Qiao , Liu Fei . Stabilized Rh/hydroxyapatite Catalyst for Furfuryl Alcohol Hydrogenation: Application of Oxidative Strong Metal-Support Interactions in Reducing Conditions. Acta Physico-Chimica Sinica, 2025, 41(4): 2408004-0. doi: 10.3866/PKU.WHXB202408004
6. [6]
  Jingke LIU , Jia CHEN , Yingchao HAN . Nano hydroxyapatite stable suspension system: Preparation and cobalt adsorption performance. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1763-1774. doi: 10.11862/CJIC.20240060
7. [7]
  Huiwei Ding , Bo Peng , Zhihao Wang , Qiaofeng Han . Advances in Metal or Nonmetal Modification of Bismuth-Based Photocatalysts. Acta Physico-Chimica Sinica, 2024, 40(4): 2305048-0. doi: 10.3866/PKU.WHXB202305048
8. [8]
  Yukai Jiang , Yihan Wang , Yunkai Zhang , Yunping Wei , Ying Ma , Na Du . Characterization and Phase Diagram of Surfactant Lyotropic Liquid Crystal. University Chemistry, 2024, 39(4): 114-118. doi: 10.3866/PKU.DXHX202309033
9. [9]
  Congying Lu , Fei Zhong , Zhenyu Yuan , Shuaibing Li , Jiayao Li , Jiewen Liu , Xianyang Hu , Liqun Sun , Rui Li , Meijuan Hu . Experimental Improvement of Surfactant Interface Chemistry: An Integrated Design for the Fusion of Experiment and Simulation. University Chemistry, 2024, 39(3): 283-293. doi: 10.3866/PKU.DXHX202308097
10. [10]
  Feiyang Liu , Liuhong Song , Miaoyu Fu , Zhi Zheng , Gang Xie , Junlong Zhao . Tryptophan’s Employment Journey. University Chemistry, 2024, 39(9): 16-21. doi: 10.12461/PKU.DXHX202404037
11. [11]
  Yi Yang , Xin Zhou , Miaoli Gu , Bei Cheng , Zhen Wu , Jianjun Zhang . Femtosecond transient absorption spectroscopy investigation on ultrafast electron transfer in S-scheme ZnO/CdIn₂S₄ photocatalyst for H₂O₂ production and benzylamine oxidation. Acta Physico-Chimica Sinica, 2025, 41(6): 100064-0. doi: 10.1016/j.actphy.2025.100064
12. [12]
  Ruiqin Feng , Ye Fan , Yun Fang , Yongmei Xia . Strategy for Regulating Surface Protrusion of Gold Nanoflowers and Their Surface-Enhanced Raman Scattering. Acta Physico-Chimica Sinica, 2024, 40(4): 2304020-0. doi: 10.3866/PKU.WHXB202304020
13. [13]
  Hong Lu , Yidie Zhai , Xingxing Cheng , Yujia Gao , Qing Wei , Hao Wei . Advancements and Expansions in the Proline-Catalyzed Asymmetric Aldol Reaction. University Chemistry, 2024, 39(5): 154-162. doi: 10.3866/PKU.DXHX202310074
14. [14]
  Xiaosong PU , Hangkai WU , Taohong LI , Huijuan LI , Shouqing LIU , Yuanbo HUANG , Xuemei LI . Adsorption performance and removal mechanism of Cd(Ⅱ) in water by magnesium modified carbon foam. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1537-1548. doi: 10.11862/CJIC.20240030
15. [15]
  Yan Xin , Yunnian Ge , Zezhong Li , Qiaobao Zhang , Huajun Tian . Research Progress on Modification Strategies of Organic Electrode Materials for Energy Storage Batteries. Acta Physico-Chimica Sinica, 2024, 40(2): 2303060-0. doi: 10.3866/PKU.WHXB202303060
16. [16]
  Xuejiao Wang , Suiying Dong , Kezhen Qi , Vadim Popkov , Xianglin Xiang . Photocatalytic CO₂ Reduction by Modified g-C₃N₄. Acta Physico-Chimica Sinica, 2024, 40(12): 2408005-0. doi: 10.3866/PKU.WHXB202408005
17. [17]
  Dan Li , Hui Xin , Xiaofeng Yi . Comprehensive Experimental Design on Ni-based Catalyst for Biofuel Production. University Chemistry, 2024, 39(8): 204-211. doi: 10.3866/PKU.DXHX202312046
18. [18]
  Limei CHEN , Mengfei ZHAO , Lin CHEN , Ding LI , Wei LI , Weiye HAN , Hongbin WANG . Preparation and performance of paraffin/alkali modified diatomite/expanded graphite composite phase change thermal storage material. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 533-543. doi: 10.11862/CJIC.20230312
19. [19]
  Bao Jia , Yunzhe Ke , Shiyue Sun , Dongxue Yu , Ying Liu , Shuaishuai Ding . Innovative Experimental Teaching for the Preparation and Modification of Conductive Organic Polymer Thin Films in Undergraduate Courses. University Chemistry, 2024, 39(10): 271-282. doi: 10.12461/PKU.DXHX202404121
20. [20]
  Xiaotian ZHU , Fangding HUANG , Wenchang ZHU , Jianqing ZHAO . Layered oxide cathode for sodium-ion batteries: Surface and interface modification and suppressed gas generation effect. Chinese Journal of Inorganic Chemistry, 2025, 41(2): 254-266. doi: 10.11862/CJIC.20240260

Get Citation

PDF

XML

Metrics

PDF Downloads(455)
Abstract views(682)
HTML views(20)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142