Citation: GONG Wei, NIU Qiong, NIU He-Lin, HU Lin, MAO Chang-Jie, SONG Ji-Ming, ZHANG Sheng-Yi, ZHENG Jun, CHEN Qian-Wang. Synthesis, Structure and Properties of a Porous Ni(Ⅱ) Coordination Polymer Constructed from 1,1'-(1,4-Butanediyl)bis(imidazole) and o-Phthalate Acid[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(3): 642-648. doi: 10.3969/j.issn.1001-4861.2013.00.115
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A coordination polymer [Ni(Pht)(bbim-4)]n (Pht=o-phthalate acid anion,bbim-4=1, 1'-(1, 4-butanediyl)bis(imidazole) was synthesized by hydrothermal reaction and characterized by elemental analysis, powder X-ray diffraction, TGA and X-ray single crystal diffraction. The crystal belongs to monoclinic system, space group C2/c. Coordination polymer [Ni(Pht)(bbim-4)]n is a three-dimensional porous coordination polymer with triangular channels. The coordination polymer shows an overall ferromagnetic behavior. Gas sorption studies suggest that the coordination polymer has selectivity in adsorption of N2 and CO2 gas. CCDC: 818068.
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