Citation: GONG Wei, NIU Qiong, NIU He-Lin, HU Lin, MAO Chang-Jie, SONG Ji-Ming, ZHANG Sheng-Yi, ZHENG Jun, CHEN Qian-Wang. Synthesis, Structure and Properties of a Porous Ni(Ⅱ) Coordination Polymer Constructed from 1,1'-(1,4-Butanediyl)bis(imidazole) and o-Phthalate Acid[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(3): 642-648. doi: 10.3969/j.issn.1001-4861.2013.00.115 shu

Synthesis, Structure and Properties of a Porous Ni(Ⅱ) Coordination Polymer Constructed from 1,1'-(1,4-Butanediyl)bis(imidazole) and o-Phthalate Acid

  • Received Date: 29 April 2012
    Available Online: 23 October 2012

    Fund Project: 国家自然科学基金(Nos.20905001, 21071002) (Nos.20905001, 21071002)安徽省自然科学基金(Nos.KJ2010A014) 和安徽大学“211”创新团队资助项目。 (Nos.KJ2010A014)

  • A coordination polymer [Ni(Pht)(bbim-4)]n (Pht=o-phthalate acid anion,bbim-4=1, 1'-(1, 4-butanediyl)bis(imidazole) was synthesized by hydrothermal reaction and characterized by elemental analysis, powder X-ray diffraction, TGA and X-ray single crystal diffraction. The crystal belongs to monoclinic system, space group C2/c. Coordination polymer [Ni(Pht)(bbim-4)]n is a three-dimensional porous coordination polymer with triangular channels. The coordination polymer shows an overall ferromagnetic behavior. Gas sorption studies suggest that the coordination polymer has selectivity in adsorption of N2 and CO2 gas. CCDC: 818068.
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