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Citation: YIN Fu-Jun, ZHAO Hong, XU Xing-You, YANG Xu-Jie. Synthesis, Structure, Properties of a Two-Dimensional Manganese(Ⅱ) Coordination Polymer with α-Naphthylacetic Acid[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(3): 589-594. doi: 10.3969/j.issn.1001-4861.2013.00.081 shu

Synthesis, Structure, Properties of a Two-Dimensional Manganese(Ⅱ) Coordination Polymer with α-Naphthylacetic Acid

  • 1.

    1. School of Chemical Engineering, Nanjing University of Science and Technology, Nanjing 210094, China;

  • Received Date: 2 May 2012
    Available Online: 15 October 2012

    Fund Project: 江苏省海洋资源开发研究院自然科学基金(JSIMR11B03)资助项目。 (JSIMR11B03)

  • The two-dimensional coordination polymer, [Mn(NAA)2(H2O)2]n (1) (HNAA=α-naphthylacetic acid) has been synthesized and characterized by single-crystal X- ray diffraction studies, elemental analysis and FTIR spectrum. Structural determination reveals that it crystallizes in monoclinic space group C2/c. Crystal data: a=3.713 3 (5) nm, b=0.625 4(5) nm, c=0.889 7(5) nm; β=99.706 (5)°, Z=4. Each Mn(Ⅱ) atom is six-coordinated with a distorted octahedral geometry. The NAA- anion acts as a μ2- bridge linking Mn(Ⅱ) atoms generating a two-dimensional network with (4, 4) topology, which are further bridged to form three-dimensional supramolecular structure by C-H…O hydrogen bonding and C-H…π interactions. The thermal stability,luminescence property and antibacterial activity of 1 were investigated. CCDC: 847386.
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