Citation: Xiaofeng Zhu, Bingbing Xiao, Jiaxin Su, Shuai Wang, Qingran Zhang, Jun Wang. Transition Metal Oxides/Chalcogenides for Electrochemical Oxygen Reduction into Hydrogen Peroxides[J]. Acta Physico-Chimica Sinica, ;2024, 40(12): 240700. doi: 10.3866/PKU.WHXB202407005 shu

Transition Metal Oxides/Chalcogenides for Electrochemical Oxygen Reduction into Hydrogen Peroxides

Xiaofeng Zhu ^1,2,, ,
Bingbing Xiao ^1,2 ,
Jiaxin Su ^1,2 ,
Shuai Wang ³ ,
Qingran Zhang ^3,, ,
Jun Wang ^1,2,,

1.
State Key Laboratory of Environment-Friendly Energy Materials, School of Materials and Chemistry, Southwest University of Science and Technology, Mianyang 621010, Sichuan Province, China;
2.
Tianfu Institute of Research and Innovation, Southwest University of Science and Technology, Chengdu 610299, China;
3.
State Key Laboratory of Pollution Control and Resources Reuse, Shanghai Institute of Pollution Control and Ecological Security, School of Environmental Science and Engineering, Tongji University, Shanghai 200092, China

Corresponding author: Xiaofeng Zhu, Qingran Zhang, Jun Wang,
Received Date: 7 July 2024
Revised Date: 3 August 2024
Accepted Date: 3 August 2024

Fund Project: The work was supported by the National Natural Science Foundation of China (52202305, 22176155), National Natural Science Foundation of Sichuan Province, China (2023NSFSC0095), Outstanding Youth Talents of Sichuan Science and Technology Program (22JCQN0061), Long Shan Talents Plan of SWUST (22zx7103), and Scientific Research Foundation for the Returned Overseas Chinese Scholars, Department of Human Resource and Social Security of Sichuan Province (22zd3148).

Electrochemical oxygen reduction reaction via the two-electron pathway (2e-ORR) is becoming a promising and sustainable approach to producing hydrogen peroxide (H₂O₂) without significant carbon footprints. To achieve better performance, most of the recent progress and investigations have focused on developing novel carbon-based electrocatalysts. Nevertheless, the sophisticated preparations, decreased selectivity and undefined active sites of carbon-based catalysts have been generally acknowledged and criticized. To this end, transition metal oxides and chalcogenides have increasingly emerged for 2e-ORR, due to their catalytic stability and tunable microstructure. Here, the development of metal oxides and chalcogenides for O₂-to-H₂O₂ conversion is prospectively reviewed. By summarizing previous theoretical and experimental efforts, their diversity and outstanding catalytic activity are firstly provided. Meanwhile, the topological and chemical factors influencing 2e-ORR selectivity of the metal oxides/chalcogenides are systematically elucidated, including morphology, phase structures, doping and defects engineering. Thus, emphasizing the influence on the binding of ORR intermediates, the active sites and the underlying mechanism is highlighted. Finally, future opportunities and challenges in designing metal oxides/chalcogenides-based catalysts for H₂O₂ electro-synthesis are outlined. The present review provides insights and fundamentals of metal oxides/chalcogenides as 2e-ORR catalysts, promoting their practical application in the energy-related industry.
- Oxides,
- Chalcogenides,
- Oxygen reduction reaction,
- H₂O₂ electro-synthesis,
- Active sites
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