Citation: ZHU Fu-Liang, CHEN Yuan-Feng, CHENG Yong-Liang, ZHU Yu-Qing, YAN Xing-Bin. Fabrication and Magnetic Properties of Electrospun Zinc Ferrite Hollow Fibers[J]. Acta Physico-Chimica Sinica, ;2012, 28(05): 1265-1268. doi: 10.3866/PKU.WHXB201202291 shu

Fabrication and Magnetic Properties of Electrospun Zinc Ferrite Hollow Fibers

1.
1. School of Material Science and Engineering, Lanzhou University of Technology, Lanzhou 730050, P. R. China;
2. State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, P. R. China

Received Date: 10 November 2011
Available Online: 29 February 2012
Fund Project: 甘肃省自然科学基金(3ZS042-B25-029) (3ZS042-B25-029)国家自然科学基金(51005225)资助项目 (51005225)

Zinc ferrite (ZnFe₂O₄) hollow fibers have been fabricated by annealing electrospun polyvinylpyrrolidone (PVP)/nitrate salt composite nanofibers at 500 °C for 3 h with a heating rate of 5 °C· min^-1. The composite fibers were initially prepared by electrospinning Zn, Fe salts, and PVP from solution. The structure, morphology, and magnetic properties were studied by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and vibrating sample magnetometry (VSM). The XRD results indicate a spinel phase structure, while SEM and TEM reveal hollow fibers (200-400 nm in diameter) with walls consisting of packed 25 nm nanoparticles. Room temperature VSM of the ZnFe₂O₄ hollow fibers reveal a superparamagnetic behavior and a magnetization value of 2.03 emu·g^-1 at 10 kOe.
- Fiber technology,
- ZnFe₂O₄,
- Hollow fiber,
- Nanoparticle,
- Magnetic property
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沈阳化工大学材料科学与工程学院沈阳 110142