Citation: ZHU Fu-Liang, CHEN Yuan-Feng, CHENG Yong-Liang, ZHU Yu-Qing, YAN Xing-Bin. Fabrication and Magnetic Properties of Electrospun Zinc Ferrite Hollow Fibers[J]. Acta Physico-Chimica Sinica, ;2012, 28(05): 1265-1268. doi: 10.3866/PKU.WHXB201202291 shu

Fabrication and Magnetic Properties of Electrospun Zinc Ferrite Hollow Fibers

1.
1. School of Material Science and Engineering, Lanzhou University of Technology, Lanzhou 730050, P. R. China;
2. State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, P. R. China

Received Date: 10 November 2011
Available Online: 29 February 2012
Fund Project: 甘肃省自然科学基金(3ZS042-B25-029) (3ZS042-B25-029)国家自然科学基金(51005225)资助项目 (51005225)

Zinc ferrite (ZnFe₂O₄) hollow fibers have been fabricated by annealing electrospun polyvinylpyrrolidone (PVP)/nitrate salt composite nanofibers at 500 °C for 3 h with a heating rate of 5 °C· min^-1. The composite fibers were initially prepared by electrospinning Zn, Fe salts, and PVP from solution. The structure, morphology, and magnetic properties were studied by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and vibrating sample magnetometry (VSM). The XRD results indicate a spinel phase structure, while SEM and TEM reveal hollow fibers (200-400 nm in diameter) with walls consisting of packed 25 nm nanoparticles. Room temperature VSM of the ZnFe₂O₄ hollow fibers reveal a superparamagnetic behavior and a magnetization value of 2.03 emu·g^-1 at 10 kOe.
- Fiber technology,
- ZnFe₂O₄,
- Hollow fiber,
- Nanoparticle,
- Magnetic property
1. [1]
  (1) Liu, Z.; Sun, X. M.; Nozomi, N. R.; Dai, H. J. ACS Nano 2007, 1, 50.
2. [2]
  (2) Gabelman, A.; Hwang, S. T. J. Membrane Sci. 1999, 159, 61.
3. [3]
  (3) Li, X. Y.; Hou, Y.; Zhao, Q. D.; Teng,W.; Hu, X. J.; Chen, G. H. Chemosphere 2011, 82, 581.
4. [4]
  (4) Leo, A.; Smart, S.; Liu, S. M.; Costa, J. D. J. Membrane Sci. 2011, 368, 64.
5. [5]
  (5) Wolfe, S. P.; Hsu, E.; Reid, L. M.; MacDonald, J. M. Biotechnol. Bioeng. 2002, 77, 83.
6. [6]
  (6) Droushiotis, N.; Doraswami, U.; Kanawka, K.; Kelsall, G. H.; Li, K. Solid State Ionics 2009, 180, 1091.
7. [7]
  (7) Say, R.; Serap, S.; Denizli, A. J. Appl. Polym. Sci. 2002, 83, 3089.
8. [8]
  (8) Qiu, P. H.; Mao, C. B. ACS Nano 2010, 4, 1573.
9. [9]
  (9) Meng, Q.;Wu, D. Q.; Zhang, G. L.; Qiu, H. X. Biotechnol. Lett. 2006, 28, 279.
10. [10]
  (10) Song, P.;Wang, Q.; Zhang, Z.; Yang, Z. X. Sensor Actuat. B-Chem. 2010, 147, 248.
11. [11]
  (11) Ge, Q. Q.;Wang, Z. B.; Yan, Y. S. J. Am. Chem. Soc. 2009, 131, 17056.
12. [12]
  (12) Fan, H. M.; Yi, J. B.; Yang, Y.; Kho, K.W.; Tan, H. R.; Shen, Z. X.; Ding, J.; Sun, X.W.; Olivo, M. C.; Feng, Y. P. ACS Nano 2009, 3, 2798.
13. [13]
  (13) Zeng, Y.; Liu, J. T.;Wu,W.; Ding, C. X. Surf. Coat. Tech. 2005, 200, 2398.
14. [14]
  (14) Yeary, L.W.; Moon, J.W.; Rawn, C. J.; Love, L. J.; Rondinone, A. J.; Thompson, J. R. J. Magn. Magn. Mater. 2011, 323, 3043.
15. [15]
  (15) Niu, X. S.; Du,W. P.; Du,W. M. Sensor Actuat B-Chem. 2004, 99, 405.
16. [16]
  (16) Deng, Y. F.; Zhang, Q. M.; Tang, S. D.; Zhang, L. T.; Deng, S. N.; Shi, Z. C. Chem. Commun. 2011, 47, 6828.
17. [17]
  (17) Atif, M.; Hasanain, S. K.; Nadeem, M. Solid State Commun. 2006, 38, 416.
18. [18]
  (18) Yuan, Z. H.; Zhang, L. D. J. Mater. Chem. 2001, 11, 1265.
19. [19]
  (19) Ehrhardt, H.; Campbell, S. J.; Hofmann, M. J. Alloy. Compd. 2002, 339, 255.
20. [20]
  (20) Naseri, M. G.; Saion, E. B.; Hashim, M.; Shaari, A. H.; Ahangar, H. A. Solid State Commun. 2011, 151, 1031.
21. [21]
  (21) Renaker, D. H.; Chun, I. Nanotechnology 1996, 7, 216.
22. [22]
  (22) Chang, G. Q.; Zheng, X.; Chen, R. Y.; Chen, X.; Chen, L. Q.; Chen, Z. Acta Phys. -Chim. Sin. 2008, 24, 1790. [常国庆, 郑曦, 陈日耀, 陈晓, 陈力勤, 陈震. 物理化学学报, 2008, 24, 1790.]
23. [23]
  (23) Ponhan,W.; Swatsitang, E.; Maensiri, S. Mater. Sci. Technol. 2010, 26, 1298.
24. [24]
  (24) Zhan, S. H.; ng, C. R.; Chen, D. R.; Jiao, X. L. J. Disper. Sci. Technol. 2006, 27, 931.
25. [25]
  (25) Cheng, Y. L.; Zou, B. L.; Yang, J. L.;Wang, C. J.; Liu, Y. J.; Cao, X. Q. Cryst. Eng. Commun. 2010, 13, 2268.
1. [1]
  Juan WANG , Zhongqiu WANG , Qin SHANG , Guohong WANG , Jinmao LI . NiS and Pt as dual co-catalysts for the enhanced photocatalytic H₂ production activity of BaTiO₃ nanofibers. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1719-1730. doi: 10.11862/CJIC.20240102
2. [2]
  Jiahong ZHENG , Jingyun YANG . Preparation and electrochemical properties of hollow dodecahedral CoNi₂S₄ supported by MnO₂ nanowires. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1881-1891. doi: 10.11862/CJIC.20240170
3. [3]
  Qin ZHU , Jiao MA , Zhihui QIAN , Yuxu LUO , Yujiao GUO , Mingwu XIANG , Xiaofang LIU , Ping NING , Junming GUO . Morphological evolution and electrochemical properties of cathode material LiAl_0.08Mn_1.92O₄ single crystal particles. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1549-1562. doi: 10.11862/CJIC.20240022
4. [4]
  Chenye An , Abiduweili Sikandaier , Xue Guo , Yukun Zhu , Hua Tang , Dongjiang Yang . 红磷纳米颗粒嵌入花状CeO₂分级S型异质结高效光催化产氢. Acta Physico-Chimica Sinica, 2024, 40(11): 2405019-. doi: 10.3866/PKU.WHXB202405019
5. [5]
  Xiaoning TANG , Junnan LIU , Xingfu YANG , Jie LEI , Qiuyang LUO , Shu XIA , An XUE . Effect of sodium alginate-sodium carboxymethylcellulose gel layer on the stability of Zn anodes. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1452-1460. doi: 10.11862/CJIC.20240191
6. [6]
  Siyu HOU , Weiyao LI , Jiadong LIU , Fei WANG , Wensi LIU , Jing YANG , Ying ZHANG . Preparation and catalytic performance of magnetic nano iron oxide by oxidation co-precipitation method. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1577-1582. doi: 10.11862/CJIC.20230469
7. [7]
  Shijie Li , Ke Rong , Xiaoqin Wang , Chuqi Shen , Fang Yang , Qinghong Zhang . Design of Carbon Quantum Dots/CdS/Ta₃N₅ S-Scheme Heterojunction Nanofibers for Efficient Photocatalytic Antibiotic Removal. Acta Physico-Chimica Sinica, 2024, 40(12): 2403005-. doi: 10.3866/PKU.WHXB202403005
8. [8]
  Qingtang ZHANG , Xiaoyu WU , Zheng WANG , Xiaomei WANG . Performance of nano Li₂FeSiO₄/C cathode material co-doped by potassium and chlorine ions. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1689-1696. doi: 10.11862/CJIC.20240115
9. [9]
  Hailang JIA , Hongcheng LI , Pengcheng JI , Yang TENG , Mingyun GUAN . Preparation and performance of N-doped carbon nanotubes composite Co₃O₄ as oxygen reduction reaction electrocatalysts. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 693-700. doi: 10.11862/CJIC.20230402
10. [10]
  Kun WANG , Wenrui LIU , Peng JIANG , Yuhang SONG , Lihua CHEN , Zhao DENG . Hierarchical hollow structured BiOBr-Pt catalysts for photocatalytic CO₂ reduction. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1270-1278. doi: 10.11862/CJIC.20240037
11. [11]
  Guoqiang Chen , Zixuan Zheng , Wei Zhong , Guohong Wang , Xinhe Wu . 熔融中间体运输导向合成富氨基g-C₃N₄纳米片用于高效光催化产H₂O₂. Acta Physico-Chimica Sinica, 2024, 40(11): 2406021-. doi: 10.3866/PKU.WHXB202406021
12. [12]
  Guangming YIN , Huaiyao WANG , Jianhua ZHENG , Xinyue DONG , Jian LI , Yi'nan SUN , Yiming GAO , Bingbing WANG . Preparation and photocatalytic degradation performance of Ag/protonated g-C₃N₄ nanorod materials. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1491-1500. doi: 10.11862/CJIC.20240086
13. [13]
  Endong YANG , Haoze TIAN , Ke ZHANG , Yongbing LOU . Efficient oxygen evolution reaction of CuCo₂O₄/NiFe-layered bimetallic hydroxide core-shell nanoflower sphere arrays. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 930-940. doi: 10.11862/CJIC.20230369
14. [14]
  Yi YANG , Shuang WANG , Wendan WANG , Limiao CHEN . Photocatalytic CO₂ reduction performance of Z-scheme Ag-Cu₂O/BiVO₄ photocatalyst. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 895-906. doi: 10.11862/CJIC.20230434
15. [15]
  Heng Chen , Longhui Nie , Kai Xu , Yiqiong Yang , Caihong Fang . 两步焙烧法制备大比表面积和结晶性增强超薄g-C₃N₄纳米片及其高效光催化产H₂O₂. Acta Physico-Chimica Sinica, 2024, 40(11): 2406019-. doi: 10.3866/PKU.WHXB202406019
16. [16]
  Min LI , Xianfeng MENG . Preparation and microwave absorption properties of ZIF-67 derived Co@C/MoS₂ nanocomposites. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1932-1942. doi: 10.11862/CJIC.20240065
17. [17]
  Yipeng Zhou , Chenxin Ran , Zhongbin Wu . Metacognitive Enhancement in Diversifying Ideological and Political Education within Graduate Course: A Case Study on “Solar Cell Performance Enhancement Technology”. University Chemistry, 2024, 39(6): 151-159. doi: 10.3866/PKU.DXHX202312096
18. [18]
  Guimin ZHANG , Wenjuan MA , Wenqiang DING , Zhengyi FU . Synthesis and catalytic properties of hollow AgPd bimetallic nanospheres. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 963-971. doi: 10.11862/CJIC.20230293
19. [19]
  Yuhao SUN , Qingzhe DONG , Lei ZHAO , Xiaodan JIANG , Hailing GUO , Xianglong MENG , Yongmei GUO . Synthesis and antibacterial properties of silver-loaded sod-based zeolite. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 761-770. doi: 10.11862/CJIC.20230169
20. [20]
  Jingke LIU , Jia CHEN , Yingchao HAN . Nano hydroxyapatite stable suspension system: Preparation and cobalt adsorption performance. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1763-1774. doi: 10.11862/CJIC.20240060

Get Citation

PDF

XML

Metrics

PDF Downloads(776)
Abstract views(2264)
HTML views(9)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142