Citation: WANG Dan-Li, RUAN Yong-Feng, ZHANG Ling-Cui, YANG Hong-Bo. Preparation by Electrodeposition and Characterization of ZnO Nanowire Arrays[J]. Acta Physico-Chimica Sinica, ;2010, 26(12): 3369-3372. doi: 10.3866/PKU.WHXB20101202 shu

Preparation by Electrodeposition and Characterization of ZnO Nanowire Arrays

1.
School of Science, Tianjin University, Tianjin 300072, P. R. China

Received Date: 30 August 2010
Available Online: 22 October 2010
Fund Project: 天津市自然科学基金(07JCZDJC00600, 07JCYBJC06000)资助项目 (07JCZDJC00600, 07JCYBJC06000)

Ordered zinc (Zn) nanowire arrays embedded in anodic aluminum oxide (AAO) templates were prepared by an effective electrodeposition method. Oxygen was used to oxidize the electrodeposited zinc nanowire arrays in the AAO templates. By thermal treatment in an oxygen atmosphere at 800 °C for 2 h, the deposited Zn was completely oxidized. The microstructures and optical properties of the synthesized zinc oxide (ZnO) nanowire arrays were investigated by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and photoluminescence (PL) spectrum analytic apparatus. We found that large scale polycrystalline ZnO nanowire arrays were uniformly assembled in the nanochannels of the AAO template. The nanowires have a very high aspect ratio of about 1000:1 with the length equaling the template thickness and a diameter of about 80 nm. PL measurements of the ZnO/AAO assembly showed a strong green emission at 504 nm, which was attributed to the oxygen vacancy defects of the ZnO nanowires. These results can be used in further studies of the structural and functional properties of electroluminescence devices based on the ZnO/AAO assembly.
- Anodic aluminum oxide,
- Zinc oxide,
- Nanowire array,
- Electrodeposition,
- Oxidization
1. [1]
  
  1. Serrano, J.; Manjón, F. J.; Romero, A. H.; Ivanov, A.; Cardona, .; Lauck, R.; Bosak, A.; Krisch, M. Phys. Rev. B, 2010, 81:174304
2. [2]
  2. Wang, Z. H.; Geng, D. Y.; Han, Z.; Zhang, Z. D. Materials etters, 2009, 63: 2533
3. [3]
  3. Willander, M.; Nur, O.; Zhao, Q. X. Nanotechnology, 2009, 20:332001
4. [4]
  4. Wang, X. Y.; Dong, G. F.; Qiao, J.;Wang, L. D.; Qiu, Y. Acta hys. -Chim. Sin., 2010, 26: 249. [王小燕, 董桂芳, 乔娟, 立铎, 邱勇. 物理化学学报, 2010, 26: 249]
5. [5]
  5. Zheng, K. B.; Li, J. L.; Shen, H. T.; Sun, D. L.; Chen, G. R. Acta hys. -Chim. Sin., 2008, 24: 1080. [郑凯波, 李静雷, 沈浩颋, 大林, 陈国荣. 物理化学学报, 2008, 24: 1080]
6. [6]
  6. Silva, C.; Costa, A. R. G.; Cruz, M. M.; da Silva, R. C.; Borges, . P.; Alves, L. C.; dinho, M. J. Phys.-Condens. Matter, 2010,22: 346005
7. [7]
  7. He, H.; Lao, C. S.; Chen, L. J.; Davidovic, D.;Wang, Z. L. J. Am. hem. Soc., 2005, 127: 16376
8. [8]
  8. Ruan, Y. F.; Yang, H. B.; Jing, H. Q.; Lü, X. Y. The novel nO-based electroluminescent device prepared by using AAO emplate: China, ZL200620027253.9. [P]. 2007-9-12. [阮永丰, 红波, 井红旗, 吕小燕. 利用多孔氧化铝模板制作的氧化锌电发光器件: 中国, ZL200620027253.9. [P]. 2007-9-12]
9. [9]
  9. Wang, D. L.; Ruan, Y. F.; Yang, H. B.; Zhang, L. C.; He, L. ournal of Synthetic Crystals, 2009, 38: 83. [王丹丽, 阮永丰, 红波, 张灵翠, 何丽. 人工晶体学报, 2009, 38: 83]
10. [10]
  10. Yang, L.; Tang, Y. H.; Chen, X. H.; Li, Y.; Cao, X. L. Mater. hem. Phys., 2007, 101: 195
11. [11]
  11. Wang, Y. C.; Ieu, I. C.; Hon, M. H. Electrochem. Solid-State Lett., 2002, 5: C53
12. [12]
  12. Zheng, M. J.; Zhang, L. D.; Li, G. H.; Shen,W. Z. Chem. Phys. ett., 2002, 363: 123
13. [13]
  13. Peulon, S.; Lincot, D. J. Electrochem. Soc., 1998, 145: 864
14. [14]
  14. Zhou, H.; Alves, H.; Hofmann, D. M.; Kriegseis,W.; Meyer, B. .; Kaczmarczyk, G.; Hoffmann, A. Appl. Phys. Lett., 2002, 80: 210
15. [15]
  15. Li, Y.; Meng, G.W.; Zhang, L. D.; Phillipp, F. Appl. Phys. Lett., 2000, 76: 2011
16. [16]
  16. Li, A. P.; Müller, F.; Birner, A.; Nielsch, K.; Güsele, U. J. Appl. hys., 1998, 84: 6023
17. [17]
  17. Yue, S.; Du, J.; Zhang, Y.; Chen, D. P. Mod. Phys. Lett. B, 2009, 23: 3497
18. [18]
  18. Kirchner, A.; MacKenzie, K. J. D.; Brown, I.W. M.; Kemmitt, T.; owden, M. E. J. Membr. Sci., 2007, 287: 264
19. [19]
  19. Vanheusden, K.; Seager, C. H.;Warren,W. L.; Tallant, D. R.; oigt, J. A. Appl. Phys. Lett., 1996, 68: 403
1. [1]
  Zijian Jiang , Yuang Liu , Yijian Zong , Yong Fan , Wanchun Zhu , Yupeng Guo . Preparation of Nano Zinc Oxide by Microemulsion Method and Study on Its Photocatalytic Activity. University Chemistry, 2024, 39(5): 266-273. doi: 10.3866/PKU.DXHX202311101
2. [2]
  Yu Wang , Shoulei Zhang , Tianming Lv , Yan Su , Xianyu Liu , Fuping Tian , Changgong Meng . Introduce a Comprehensive Inorganic Synthesis Experiment: Synthesis of Nano Zinc Oxide via Microemulsion Using Waste Soybean Oil. University Chemistry, 2024, 39(7): 316-321. doi: 10.3866/PKU.DXHX202311035
3. [3]
  Endong YANG , Haoze TIAN , Ke ZHANG , Yongbing LOU . Efficient oxygen evolution reaction of CuCo₂O₄/NiFe-layered bimetallic hydroxide core-shell nanoflower sphere arrays. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 930-940. doi: 10.11862/CJIC.20230369
4. [4]
  Shicheng Yan . Experimental Teaching Design for the Integration of Scientific Research and Teaching: A Case Study on Organic Electrooxidation. University Chemistry, 2024, 39(11): 350-358. doi: 10.12461/PKU.DXHX202408036
5. [5]
  Ping ZHANG , Chenchen ZHAO , Xiaoyun CUI , Bing XIE , Yihan LIU , Haiyu LIN , Jiale ZHANG , Yu'nan CHEN . Preparation and adsorption-photocatalytic performance of ZnAl@layered double oxides. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1965-1974. doi: 10.11862/CJIC.20240014
6. [6]
  Xiaoning TANG , Shu XIA , Jie LEI , Xingfu YANG , Qiuyang LUO , Junnan LIU , An XUE . Fluorine-doped MnO₂ with oxygen vacancy for stabilizing Zn-ion batteries. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1671-1678. doi: 10.11862/CJIC.20240149
7. [7]
  Xiaomei Ning , Liang Zhan , Xiaosong Zhou , Jin Luo , Xunfu Zhou , Cuifen Luo . Preparation and Electro-Oxidation Performance of PtBi Supported on Carbon Cloth: A Recommended Comprehensive Chemical Experiment. University Chemistry, 2024, 39(11): 217-224. doi: 10.3866/PKU.DXHX202401085
8. [8]
  Siyu HOU , Weiyao LI , Jiadong LIU , Fei WANG , Wensi LIU , Jing YANG , Ying ZHANG . Preparation and catalytic performance of magnetic nano iron oxide by oxidation co-precipitation method. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1577-1582. doi: 10.11862/CJIC.20230469
9. [9]
  Chunmei GUO , Weihan YIN , Jingyi SHI , Jianhang ZHAO , Ying CHEN , Quli FAN . Facile construction and peroxidase-like activity of single-atom platinum nanozyme. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1633-1639. doi: 10.11862/CJIC.20240162
10. [10]
  Jiaxin Su , Jiaqi Zhang , Shuming Chai , Yankun Wang , Sibo Wang , Yuanxing Fang . Optimizing Poly(heptazine imide) Photoanodes Using Binary Molten Salt Synthesis for Water Oxidation Reaction. Acta Physico-Chimica Sinica, 2024, 40(12): 2408012-. doi: 10.3866/PKU.WHXB202408012
11. [11]
  Minna Ma , Yujin Ouyang , Yuan Wu , Mingwei Yuan , Lijuan Yang . Green Synthesis of Medical Chemiluminescence Reagents by Photocatalytic Oxidation. University Chemistry, 2024, 39(5): 134-143. doi: 10.3866/PKU.DXHX202310093
12. [12]
  Yunting Shang , Yue Dai , Jianxin Zhang , Nan Zhu , Yan Su . Something about RGO (Reduced Graphene Oxide). University Chemistry, 2024, 39(9): 273-278. doi: 10.3866/PKU.DXHX202306050
13. [13]
  Linbao Zhang , Weisi Guo , Shuwen Wang , Ran Song , Ming Li . Electrochemical Oxidation of Sulfides to Sulfoxides. University Chemistry, 2024, 39(11): 204-209. doi: 10.3866/PKU.DXHX202401009
14. [14]
  Chuanming GUO , Kaiyang ZHANG , Yun WU , Rui YAO , Qiang ZHAO , Jinping LI , Guang LIU . Performance of MnO₂-0.39IrO_x composite oxides for water oxidation reaction in acidic media. Chinese Journal of Inorganic Chemistry, 2024, 40(6): 1135-1142. doi: 10.11862/CJIC.20230459
15. [15]
  Zhihuan XU , Qing KANG , Yuzhen LONG , Qian YUAN , Cidong LIU , Xin LI , Genghuai TANG , Yuqing LIAO . Effect of graphene oxide concentration on the electrochemical properties of reduced graphene oxide/ZnS. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1329-1336. doi: 10.11862/CJIC.20230447
16. [16]
  Simin Fang , Wei Huang , Guanghua Yu , Cong Wei , Mingli Gao , Guangshui Li , Hongjun Tian , Wan Li . Integrating Science and Education in a Comprehensive Chemistry Design Experiment: The Preparation of Copper(I) Oxide Nanoparticles and Its Application in Dye Water Remediation. University Chemistry, 2024, 39(8): 282-289. doi: 10.3866/PKU.DXHX202401023
17. [17]
  Xiaofeng Zhu , Bingbing Xiao , Jiaxin Su , Shuai Wang , Qingran Zhang , Jun Wang . Transition Metal Oxides/Chalcogenides for Electrochemical Oxygen Reduction into Hydrogen Peroxides. Acta Physico-Chimica Sinica, 2024, 40(12): 2407005-. doi: 10.3866/PKU.WHXB202407005
18. [18]
  Kai CHEN , Fengshun WU , Shun XIAO , Jinbao ZHANG , Lihua ZHU . PtRu/nitrogen-doped carbon for electrocatalytic methanol oxidation and hydrogen evolution by water electrolysis. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1357-1367. doi: 10.11862/CJIC.20230350
19. [19]
  Zhuo WANG , Junshan ZHANG , Shaoyan YANG , Lingyan ZHOU , Yedi LI , Yuanpei LAN . Preparation and photocatalytic performance of CeO₂-reduced graphene oxide by thermal decomposition. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1708-1718. doi: 10.11862/CJIC.20240067
20. [20]
  Yongmei Liu , Lisen Sun , Zhen Huang , Tao Tu . Curriculum-Based Ideological and Political Design for the Experiment of Methanol Oxidation to Formaldehyde Catalyzed by Electrolytic Silver. University Chemistry, 2024, 39(2): 67-71. doi: 10.3866/PKU.DXHX202308020

Get Citation

PDF

XML

Metrics

PDF Downloads(2237)
Abstract views(5076)
HTML views(2)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142