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Citation: LI Li-Ying, SONG Wen-Hua, CHEN Tie-Hong. Synthesis of Hydroxyapatite Nanoplates by the Hydrothermal Reaction Method with Anionic Amino Acid Surfactant[J]. Acta Physico-Chimica Sinica, ;2009, 25(11): 2404-2408. doi: 10.3866/PKU.WHXB20091020 shu

Synthesis of Hydroxyapatite Nanoplates by the Hydrothermal Reaction Method with Anionic Amino Acid Surfactant

1.
School of Environmental and Chemical Engineering, Tianjin Polytechnic University, Tianjin 300160, P. R. China

Received Date: 1 June 2009
Available Online: 31 August 2009

By hydrothermal reaction method with the control of anionic amino acid surfactant N-lauroylsarcosine sodium (Sar-Na), single crystal hydroxyapatite (HAP) nanoplates were synthesized and different synthetic conditions were carefully studied. The products were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared (FTIR) spectroscopy. Results showed that hydroxyapatite nanocrystals with lengths of 0.5-1.0 μm, a width of 30 nm, and a high aspect ratio (20:1) were obtained. By increasing the concentration of N-lauroylsarcosine sodium, the morphology of the hydroxyapatite varied from oval to plate-like. These results show that N-lauroylsarcosine sodium can induce the formation of hydroxyapatite with different morphologies. The current work provides a new approach to tune the aspect ratio of hydroxyapatite nanoplates.
- Hydroxyapatite,
- Nanoplate,
- N-lauroylsarcosine sodium,
- Morphology,
- Aspect ratio
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