Citation: HUANG Jian-Shu, ZHANG Xiao-Gang. Microwave Synthesis of Pt-Au/MWCNTs Electrocatalyst and Its Catalytic Properties for Oxygen Reduction[J]. Acta Physico-Chimica Sinica, ;2006, 22(12): 1551-1554. doi: 10.3866/PKU.WHXB20061223
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Pt-Au/MWCNTs (multi-wall carbon nanotubes) electrocatalyst was prepared by microwave method, and characterized by SEM, TEM, and EDS techniques. The results showed that the Pt-Au nanoparticles were small and well dispersed on the surface of MWCNTs. The electrochemical behaviors were studied by rotating disk electrode (RDE) technique in 0.1 mol•L−1 HClO4 solution. The linear sweeping voltammetry (LSV) results indicated that Pt-Au/MWCNTs with mPt:mAu of 1:2 exhibited the highest catalytic activity for oxygen reduction.
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