Citation:
CAO Jie-ming, WANG Jun, FANG Bao-qing, ZHENG Ming-bo, LU Hong-xia, CHANG Xin, WANG Hai-yan. Synthesis and Characterization of ZnO Nanomaterials with Different Morphologies in Ionic Liquids[J]. Acta Physico-Chimica Sinica,
;2005, 21(06): 668-672.
doi:
10.3866/PKU.WHXB20050618
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ZnO nano/microstructures of different morphologies have been synthesized by using Zn(OH)42- and different ionic liquids with the aid of microwave irradiation. The as-prepared samples are characterized by X-ray diffraction (XRD), scanning electron microcopy (SEM), transmission electron microscopy (TEM), and photoluminescence(PL). The XRD pattern shows that the asprepared samples have hexa nal structures, SEM and TEM images demonstrate that sheet and rod aggregates of ZnO are formed. SAED(selected area electron diffraction) images of rods indicate the single crystal nature, and the PL spectrum of ZnO nanosheet aggregates exhibits a weak ultraviolet emission and a strong green emission at room temperature.
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