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Citation: Zhu Su-Bing, Sun Si-Xiu, Xu Jun-Jian, Li Yan. The Preparation of Nitrogen-doped Carbon Nanotubes from Pyridine[J]. Acta Physico-Chimica Sinica, ;2004, 20(11): 1320-1323. doi: 10.3866/PKU.WHXB20041107 shu

The Preparation of Nitrogen-doped Carbon Nanotubes from Pyridine

1.
College of Chemistry and Molecular Engineering, Peking University, Beijing　100871; College of Chemistry and Chemical Engineering, Shangdong University, Jinan　250100

Received Date: 13 April 2004
Available Online: 15 November 2004

Bamboo-like nanotubes with a diameter of 20～40 nm were prepared by thermal decomposition of pyridine at 700～800 ℃. EDX and XPS measurements show that they are nitrogen-doped carbon nanotubes. It was found that the intensity of the D band in the Raman spectrum of the N-doped tubes is much higher than that of undoped tubes. It was also found by TGA that the doped tubes were oxidized at much lower temperature. These both indicate that nitrogen-doping introduces defects into the graphite sheets of the tubes. HRTEM result is in od agreement with this.
- Pyridine;CVD;Nitrogen-doped;Bamboo-like carbon nanotubes
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