Citation: Chen Feng, Zhu Yi-Ping, Ma Hong-Liao, Bo Zi-Long, Zhang Jin-Long. Preparation and Characterization of TiO2--CdS-MCM-41 Nano-composite[J]. Acta Physico-Chimica Sinica, ;2004, 20(11): 1292-1296. doi: 10.3866/PKU.WHXB20041102
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γ-thiopropyl tri-methyl silicane and surface pre-adsorption hydrolysis technique were used to accommodate CdS and TiO2 nanoparticles into the tunnels of MCM-41 meso-porous sieves. UV-Vis spectra showed that MCM-41 extracted CdS nanoparticles effectively from the reverse micelles by the chelation of thiol-groups. The changes of meso-tunnel diameter of MCM-41 were also observed with the introducing of nanoparticles in the low angle XRD patterns.
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Keywords:
- CdS; TiO2; MCM-41; Nano-composite
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