Citation:
Yao Yun-Feng, Zhang Mai-Sheng, Yang Yan-Sheng. Synthesis of Nano-sized MCM-41 Mesoporous Molecular Sieve by[J]. Acta Physico-Chimica Sinica
doi:
10.3866/PKU.WHXB20011212
-
A rapid synthesis of mesoporous molecular sieve MCM-41 with nanometer size by sol-gel method under microwave radiation heating is reported. The effect of different factors, such as raw materials ratio, acidity, power and duration of microwave radiation employed in crystallization and removal of organic template processes on the morphology of the products was systemically investigated and the optimum reaction conditions were also selected. The resulting samples were characterized with such techniques as XRD, HRTEM, IR, TG, photoluminescence spectroscopy and N2 adsorption isotherm, etc. The results showed that reaction time and energy required in the synthesis of MCM-41 mesophase by microwave radiation method were greatly reduced in contrast with those needed by hydrothermal method. The samples, which displayed a hexa nal mesostructure with short-range order having pore diameter of about 2.5 nm exhibited a photoluminescence effect due to the nanometer-diameter crystallites(about 40 nm, see Fig.2~3). The as-prepared MCM-41 mesoporous molecular sieve was found to possess a huge surface area, pore volume and od thermal stability (see Table 3).
-
-
-
-
[1]
Jing WU , Puzhen HUI , Huilin ZHENG , Pingchuan YUAN , Chunfei WANG , Hui WANG , Xiaoxia GU . Synthesis, crystal structures, and antitumor activities of transition metal complexes incorporating a naphthol-aldehyde Schiff base ligand. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20240278
-
[2]
Xinting XIONG , Zhiqiang XIONG , Panlei XIAO , Xuliang NIE , Xiuying SONG , Xiuguang YI . Synthesis, crystal structures, Hirshfeld surface analysis, and antifungal activity of two complexes Na(Ⅰ)/Cd(Ⅱ) assembled by 5-bromo-2-hydroxybenzoic acid ligands. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20240145
-
[3]
Jiaming Xu , Yu Xiang , Weisheng Lin , Zhiwei Miao . Research Progress in the Synthesis of Cyclic Organic Compounds Using Bimetallic Relay Catalytic Strategies. University Chemistry, doi: 10.3866/PKU.DXHX202309093
-
[4]
Yufang GAO , Nan HOU , Yaning LIANG , Ning LI , Yanting ZHANG , Zelong LI , Xiaofeng LI . Nano-thin layer MCM-22 zeolite: Synthesis and catalytic properties of trimethylbenzene isomerization reaction. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20240036
-
[5]
Yuhao SUN , Qingzhe DONG , Lei ZHAO , Xiaodan JIANG , Hailing GUO , Xianglong MENG , Yongmei GUO . Synthesis and antibacterial properties of silver-loaded sod-based zeolite. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20230169
-
[6]
Qilu DU , Li ZHAO , Peng NIE , Bo XU . Synthesis and characterization of osmium-germyl complexes stabilized by triphenyl ligands. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20240006
-
[7]
Fei Liu , Dong-Yang Zhao , Kai Sun , Ting-Ting Yu , Xin Wang . Comprehensive Experimental Design for Photochemical Synthesis, Analysis, and Characterization of Seleno-Containing Medium-Sized N-Heterocycles. University Chemistry, doi: 10.3866/PKU.DXHX202309047
-
[8]
Aidang Lu , Yunting Liu , Yanjun Jiang . Comprehensive Organic Chemistry Experiment: Synthesis and Characterization of Triazolopyrimidine Compounds. University Chemistry, doi: 10.3866/PKU.DXHX202401029
-
[9]
Tingting Yu , Si Chen , Lianglong Sun , Tongtong Shi , Kai Sun , Xin Wang . Comprehensive Experimental Design for the Photochemical Synthesis, Analysis, and Characterization of Difluoropyrroles. University Chemistry, doi: 10.3866/PKU.DXHX202401022
-
[10]
Jiapei Zou , Junyang Zhang , Xuming Wu , Cong Wei , Simin Fang , Yuxi Wang . A Comprehensive Experiment Based on Electrocatalytic Nitrate Reduction into Ammonia: Synthesis, Characterization, Performance Exploration, and Applicable Design of Copper-based Catalysts. University Chemistry, doi: 10.3866/PKU.DXHX202312081
-
[11]
Yuena Yu , Fang Fang . Microwave-Assisted Synthesis of Safinamide Methanesulfonate. University Chemistry, doi: 10.3866/PKU.DXHX202401076
-
[12]
Kai Yang , Gehua Bi , Yong Zhang , Delin Jin , Ziwei Xu , Qian Wang , Lingbao Xing . Comprehensive Polymer Chemistry Experiment Design: Preparation and Characterization of Rigid Polyurethane Foam Materials. University Chemistry, doi: 10.3866/PKU.DXHX202308045
-
[13]
Wenjun Yang , Qiaoling Tan , Wenjiao Xie , Xiaoyu Pan , Youyong Yuan . Construction and Characterization of Calcium Alginate Microparticle Drug Delivery System: A Novel Design and Teaching Practice in Polymer Experiments. University Chemistry, doi: 10.12461/PKU.DXHX202405150
-
[14]
Pei Li , Yuenan Zheng , Zhankai Liu , An-Hui Lu . Boron-Containing MFI Zeolite: Microstructure Control and Its Performance of Propane Oxidative Dehydrogenation. Acta Physico-Chimica Sinica, doi: 10.3866/PKU.WHXB202406012
-
[15]
Jiali CHEN , Guoxiang ZHAO , Yayu YAN , Wanting XIA , Qiaohong LI , Jian ZHANG . Machine learning exploring the adsorption of electronic gases on zeolite molecular sieves. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20240408
-
[16]
Yiping HUANG , Liqin TANG , Yufan JI , Cheng CHEN , Shuangtao LI , Jingjing HUANG , Xuechao GAO , Xuehong GU . Hollow fiber NaA zeolite membrane for deep dehydration of ethanol solvent by vapor permeation. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20240224
-
[17]
Rui Gao , Ying Zhou , Yifan Hu , Siyuan Chen , Shouhong Xu , Qianfu Luo , Wenqing Zhang . Design, Synthesis and Performance Experiment of Novel Photoswitchable Hybrid Tetraarylethenes. University Chemistry, doi: 10.3866/PKU.DXHX202310050
-
[18]
Zhifang SU , Zongjie GUAN , Yu FANG . Process of electrocatalytic synthesis of small molecule substances by porous framework materials. Chinese Journal of Inorganic Chemistry, doi: 10.11862/CJIC.20240290
-
[19]
Haiyu Nie , Chenhui Zhang , Fengpei Du . Ideological and Political Design for the Preparation, Characterization and Particle Size Control Experiment of Nanoemulsion. University Chemistry, doi: 10.3866/PKU.DXHX202306055
-
[20]
Yongming Guo , Jie Li , Chaoyong Liu . Green Improvement and Educational Design in the Synthesis and Characterization of Silver Nanoparticles. University Chemistry, doi: 10.3866/PKU.DXHX202309057
-
[1]
Metrics
- PDF Downloads(3061)
- Abstract views(4587)
- HTML views(8)