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Citation: Hou Wen-Hua, Yan Qi-Jie, Fu Xian-Cai. Preparation and Characterization of Alumina-pillared Layered Titanate with a High Interlayer Spacing[J]. Acta Physico-Chimica Sinica, ;1994, 10(02): 100-102. doi: 10.3866/PKU.WHXB19940202 shu

Preparation and Characterization of Alumina-pillared Layered Titanate with a High Interlayer Spacing

1.
Department of Chemistry, Nanjing University, Nanjing 210008

Received Date: 12 October 1993
Available Online: 15 February 1994

This note mainly reports a successful preparation of a alumina-pillared layered titanate with a high interlayer spacing through a step-wise exchange process. X-ray diffeaction patterns indicate that the resultant alumina-pillared layered titanate has an interlayer spacing of 1.70 nm, which is 0.17 nm higher than that of previously reported,and has a thermal stability over 500 ℃. The surface area (N2, BET method) of the product is determined to be 72.4 m2·g-1. The N2 adsorption and desorption isotherm of the product demonstrates that the resultant alumina-pillared layered titanate is porous, with both micropores and mesopores.
- High interlayer spacing,
- Alumina-pillared Iayered titanate,
- Preparation and characterization
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