Citation: Deng Feng, Li Li-Yun, Sun Hong-Zhe, Du You-Ru. 1H MAS NMR STUDIES OF H2S AND ALCOHOLS ADSORBED ON CHARCOAL[J]. Acta Physico-Chimica Sinica, ;1990, 6(06): 648-650. doi: 10.3866/PKU.WHXB19900603
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A mag1c angle spinning system for sealed samples has been achieved with a speed from 1.5 to 4.2 kHz. Using this system, high-resolution ~1H spectra are obtained for H_2S and alcohols adsorbed on charcoal in sealed ampoules. For high coverage of alcohols, the spectral lines are resolved very well, but for low coverage, the spectral lines cannot be separated completely. The details are discussed and the solution is anticipated.
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