Abstract: Focusing on the goal of innovative talent cultivation centered on student development, we have, over years of ongoing educational reform and exploration, proposed a modular analytical chemistry experiment teaching approach based on the “comprehensive + exploratory” experiments. The undergraduates are required to independently design experimental protocols for the problems discovered during the comprehensive experiments, and then conduct individual experiment. Meanwhile, the graduate seminar mode is integrated into the experimental teaching, through the inclusion of an experimental protocol defense, finally achieving the “one student, one plan” educational strategy. Since the implementation of this teaching method, significant improvements have been observed. The approach not only stimulates students’ potential interest in learning and experiment, but also enhances integrated practical skills including experimental reasoning and knowledge application. Furthermore, it paves the way for cultivating divergent thinking and innovative capabilities, receiving widespread acclaim and endorsement.