Citation: Wei Li, Guoqiang Feng, Ze Chang. Teaching Reform of X-ray Diffraction Using Synchrotron Radiation in Materials Chemistry[J]. University Chemistry, ;2024, 39(3): 29-35. doi: 10.3866/PKU.DXHX202308060 shu

Teaching Reform of X-ray Diffraction Using Synchrotron Radiation in Materials Chemistry

Wei Li ^1,, ,
Guoqiang Feng ² ,
Ze Chang ¹

1.
School of Materials Science and Engineering, Nankai University, Tianjin 300350, China;
2.
Department of Physics and Mechanical&Electrical Engineering, Hubei University of Education, Wuhan 430205, China

Corresponding author: Wei Li, wl276@nankai.edu.cn
Received Date: 17 August 2023

X-ray diffraction is a pivotal technique for material structure analysis, playing a fundamental role in materials chemistry. In light of the continuous discovery of novel materials, advanced X-ray diffraction methods have emerged at the forefront of materials chemistry. This paper introduces a teaching reform incorporating three advanced X-ray techniques into materials chemistry instruction: high-pressure synchrotron X-ray diffraction, micro-focus X-ray diffraction, and X-ray pair distribution function analysis. We anticipate that such a teaching reform will empower students to deepen their grasp of X-ray diffraction techniques, broaden their academic horizons, and refine their problem-solving skills.
- X-ray diffraction,
- High-pressure,
- Micro-focus,
- Pair distribution function
1. [1]
2. [2]
3. [3]
  Zhang, L.; Wang, K.; Lin, Y.; Zou, B. J. Phys. Chem. Lett. 2020, 11, 4693.
4. [4]
5. [5]
  Szafrański, M.; Katrusiak, A. J. Phys. Chem. Lett. 2017, 8, 2496.
6. [6]
  Gao, F. F.; Li, X.; Qin, Y.; Li, Z. G.; Guo, T. M.; Zhang, Z. Z.; Su, G. D.; Jiang, C. Y.; Muhammad, A.; Li, W.; et al. Adv. Optical Mater. 2021, 9, 2100003.
7. [7]
  Yin, T. T.; Liu, B.; Yan, J. X.; Fang, Y. N.; Chen, M. H.; Chong, K. W.; Jiang, S. J.; Kuo, J.-L.; Fang, J. Y.; Liang, P.; et al. J. Am. Chem. Soc. 2019, 141, 1235.
8. [8]
9. [9]
  Zhang, L. L.; Yan, S.; Jiang, S.; Yang, K.; Wang, H.; He, S. M.; Liang, D. X.; Zhang, L.; He, Y.; Lan, X. Y.; et al. Nucl. Sci. Tech. 2015, 26, 3.
10. [10]
  Kikpatrick, P.; Baez, A. V. J. Opt. Soc. Am. 1948, 38, 766.
11. [11]
  An, L. C.; Li, X.; Li, Z. G.; Li, Q.; Beldon, P. J.; Gao, F. F.; Li, Z. Y.; Zhu, S. L.; Di, L.; Zhao, S. C.; et al. Nat. Commun. 2022, 13, 6645.
12. [12]
  Keen, D. A.; Goodwin, A. L. Nature 2015, 521, 303.
13. [13]
  Terban, M. W.; Billinge, S. J. L. Chem. Rev. 2022, 122, 1208.
14. [14]
  Dove, M. T.; Li, G. Nucl. Anal. 2022, 1, 2773.
15. [15]
  Haines, J.; Levelut, C.; Isambert, A.; Hebert, P.; Kohara, S.; Keen, D. A.; Hammouda, T.; Andrault, D. J. Am. Chem. Soc. 2009, 131, 12333.
16. [16]
  Bennett, T. D.; Goodwin, A. L.; Dove, M. T.; Keen, D. A.; Tucker, M. G.; Barney, E. R.; Soper, A. K.; Bithell, E. G.; Tan, J. C.; Cheetham, A. K. Phys. Rev. Lett. 2010,104, 115503.
17. [17]
  Moreno, J. J. G.; Pan, K.; Wang, Y.; Li, W. J. Langmuir 2020, 36, 5680.
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