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Citation: Tao Jiang, Yuting Wang, Lüjin Gao, Yi Zou, Bowen Zhu, Li Chen, Xianzeng Li. Experimental Design for the Preparation of Composite Solid Electrolytes for Application in All-Solid-State Batteries: Exploration of Comprehensive Chemistry Laboratory Teaching[J]. University Chemistry, ;2024, 39(2): 371-378. doi: 10.3866/PKU.DXHX202308057 shu

Experimental Design for the Preparation of Composite Solid Electrolytes for Application in All-Solid-State Batteries: Exploration of Comprehensive Chemistry Laboratory Teaching

Tao Jiang ^1,2 ,
Yuting Wang ¹ ,
Lüjin Gao ¹ ,
Yi Zou ¹ ,
Bowen Zhu ¹ ,
Li Chen ^1,, ,
Xianzeng Li ²

1.
School of Science, Tianjin University, Tianjin 300072, China;
2.
Nanjing No.1 Middle School, Nanjing 210001, China

Corresponding author: Li Chen, chenli_su@eyou.com
Received Date: 17 August 2023

A comprehensive chemistry experiment on Organic-Inorganic Composite Solid Electrolytes (SPE) is introduced, aiming to familiarize students with the modification strategies of Polyethylene Oxide (PEO) and the application of SPE in all-solid-state batteries. The experiment involves X-ray diffraction (XRD) characterization of crystal structure, as well as tests such as AC impedance, linear sweep voltammetry, and constant current charge-discharge to enhance students’ understanding of concepts such as polarization and ion migration number. This experiment helps students extend theoretical knowledge to practical applications, improves their theoretical level, and enhances their practical skills.
1. [1]
2. [2]
3. [3]
  Feng, J. N.; Wang, L.; Chen, Y. J.; Wang, P. Y.; Zhang, H. R.; He, X. M. Nano Converg. 2021, 8 (1), 1.
4. [4]
5. [5]
6. [6]
  Xiao, Z. L.; Long, T. Y.; Song, L. B.; Zheng, Y. H.; Wang, C. Ionics 2022, 28 (1), 15.
7. [7]
  Yu, X. W.; Manthiram, A. Energy Storage Mater. 2021, 34, 282.
8. [8]
9. [9]
  Chen, X. L.; Wang, T.; Lu, W. Z.; Cao, T. X.; Xue, M. Z.; Li, B.; Zhang, C. M. J. Alloy. Compd. 2018,744, 386.
10. [10]
  Zhou, D.; Mei, X. G.; Ouyang, J. Y. J. Phys. Chem. C 2011, 115, 16688.
11. [11]
12. [12]
13. [13]
1. [1]
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