变压吸附实验装置的小型化、低成本化改进

引用本文: 李清骊, 行甜雨, 杨钰欣, 王卓鹏. 变压吸附实验装置的小型化、低成本化改进[J]. 大学化学, 2024, 39(1): 173-177. doi: 10.3866/PKU.DXHX202306079 shu

Citation: Qingli Li, Tianyu Xing, Yuxin Yang, Zhuopeng Wang. Design of a Low-Cost Benchtop System for Pressure Swing Adsorption Experiments for Undergraduate Laboratory Teaching[J]. University Chemistry, 2024, 39(1): 173-177. doi: 10.3866/PKU.DXHX202306079 shu

变压吸附实验装置的小型化、低成本化改进

东北大学理学院化学系, 沈阳 110819

通讯作者: 王卓鹏,Email:wangzhuopeng@mail.neu.edu.cn

基金项目:
东北大学基本科研业务费项目（N2105012）

摘要: 目前的变压吸附实验中通常使用商品化设备，存在尺寸大、成本高、气路复杂等问题，不利于大规模开展本科实验教学。本文对变压吸附装置进行了小型化、低成本化改进，学生可以使用实验室常见材料自行搭建变压吸附装置，了解并掌握设备搭建、调试、运行的整个流程。以Li交换分子筛作为吸附剂，该设备的制氧效果与商用制氧机相当，出口氧气浓度可达95.8%。该装置具有安全性高、可反复拆装的特点，搭建、调试过程具有一定趣味性，适合用于应用化学、化学工程等本科专业的变压吸附实验教学，有利于激发学生对创制实验装置的兴趣，锻炼学生的动手能力，提高学生理论结合实际解决问题的能力。

关键词:

English

Design of a Low-Cost Benchtop System for Pressure Swing Adsorption Experiments for Undergraduate Laboratory Teaching

Department of Chemistry, College of Sciences, Northeastern University, Shenyang 110819, China

Corresponding author: Zhuopeng Wang, wangzhuopeng@mail.neu.edu.cn

Received Date: 29 June 2023

Abstract: At present, commercial systems are usually used in pressure swing adsorption (PSA) experiments. However, the purchased equipment has disadvantages such as large size, complicated tubing design and high price, which are not conducive to undergraduate laboratory teaching. In this paper, a low-cost benchtop design of PSA system is proposed, with which students can build their own PSA equipment with common laboratory materials and conduct the testing and operation on their own. Using Li-exchanged zeolite as the adsorbent, the system can produce high-purity oxygen with a concentration up to 95.8%, which is comparable to that of commercial oxygen concentrator. The designed system can be disassembled and reassembled repeatedly and the process of building and testing is safe and fun. The proposed design can be used in the PSA experimental teaching for undergraduate students who major in applied chemistry, chemical engineering and other related subjects. We believe that students' interest in creating experimental equipment can be intrigued and their ability to solve practical problems can be improved during the build and testing process of the proposed PSA system.

Key words:

1. [1]
  Ruthven, D. M.; Farooq, S.; Knaebel, K. S. Pressure Swing Adsorption; WileyVCH: New York, NY, USA, 1994.Ruthven, D. M.; Farooq, S.; Knaebel, K. S. Pressure Swing Adsorption; WileyVCH: New York, NY, USA, 1994.
2. [2]
  魏玺群, 陈健. 低温与特气, 2002, 20, 1.
3. [3]
  Sircar, S. Ind. Eng. Chem. Res. 2002, 41,1389.Sircar, S. Ind. Eng. Chem. Res. 2002, 41,1389.
4. [4]
  马江权, 魏科年, 韶晖, 冷一欣. 化工原理实验. 第3版. 武汉: 华东理工出版社, 2016: 207–212.
5. [5]
  李勇, 王世锋, 吴琪, 赵董叶, 李鑫, 周倩玉. 现代化工, 2021, 41 (8), 68.
6. [6]
  耿燕, 安生永, 王月英, 吴少帅. 河北省科学院学报, 2020, 37 (1), 51.
7. [7]
  Auerbach, S. M.; Carrado, K. A.; Dutta, P. K. Handbook of Zeolite Science and Technology, 1st ed.; Marcel Dekker Inc: Boca Raton, FL, USA, 2003, pp. 1287–1340.Auerbach, S. M.; Carrado, K. A.; Dutta, P. K. Handbook of Zeolite Science and Technology, 1st ed.; Marcel Dekker Inc: Boca Raton, FL, USA, 2003, pp. 1287–1340.
8. [8]
  Jee, J.-G.; Kim M.-B.; Lee, C.-H. Chem. Eng. Sci. 2005, 60, 869.Jee, J.-G.; Kim M.-B.; Lee, C.-H. Chem. Eng. Sci. 2005, 60, 869.
9. [9]
  卜令兵, 刘应书, 张德鑫, 刘文海. 化学工业与工程, 2007, 24 (1), 60.
10. [10]
  楼百根, 李鹏, 杨春, 孙莉, 刘文文, 钱晶. 家电科技, 2021, 3, 38.

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沈阳化工大学材料科学与工程学院沈阳 110142

变压吸附实验装置的小型化、低成本化改进

通讯作者: 王卓鹏,Email:wangzhuopeng@mail.neu.edu.cn

English

Design of a Low-Cost Benchtop System for Pressure Swing Adsorption Experiments for Undergraduate Laboratory Teaching

Corresponding author: Zhuopeng Wang, wangzhuopeng@mail.neu.edu.cn

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通讯作者: 陈斌, bchen63@163.com

中国化学会秘书处

变压吸附实验装置的小型化、低成本化改进

通讯作者: 王卓鹏,Email:wangzhuopeng@mail.neu.edu.cn

English

Design of a Low-Cost Benchtop System for Pressure Swing Adsorption Experiments for Undergraduate Laboratory Teaching

Corresponding author: Zhuopeng Wang, wangzhuopeng@mail.neu.edu.cn

CCS Chemistry：嵌段共聚物自组装成 “三明治”二维有机材料，实现纳米级压力传感功能

CCS Chemistry：颜徐州、鲍哲南： 你的皮肤可能是一片SPMs

CCS Chemistry：工作高效不疲劳，只须让催化剂动起来

CCS Chemistry：静电组装导向聚合- 聚电解质纳米凝胶量化制备新策略

CCS Chemistry：金黄色葡萄球菌醛基脱氢酶是如何识别特异性底物的？

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通讯作者: 陈斌, bchen63@163.com

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