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Citation: WANG Xiaoling, GONG Chuqing, ZHONG Yalan, HUANG Chi. Preparation of Fe₂O₃ and Fe₃O₄ Nanoparticles and the Catalytic Performance for Thermal Decomposition of Ammonium Perchlorate[J]. University Chemistry, ;2018, 33(4): 51-56. doi: 10.3866/PKU.DXHX201711002 shu

Preparation of Fe₂O₃ and Fe₃O₄ Nanoparticles and the Catalytic Performance for Thermal Decomposition of Ammonium Perchlorate

National Demonstration Center for Experimental Chemistry Education(Wuhan University), College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, P. R. China

Received Date: 1 November 2017

The Fe₃O₄ and Fe₂O₃ nanoparticles were successfully prepared by hydrothermal method. The Fe₃O₄ and Fe₂O₃ nanoparticles were characterized by X-ray powder diffraction (XRD) and the transmission electron microscopy (TEM).The obtained Fe₃O₄ and Fe₂O₃ were spheres and the diameter was about 10-20 nm. The catalysis activity of Fe₃O₄ and Fe₂O₃ on the thermal decomposition of ammonium perchlorate (AP) was appraised by thermalanalysis (TG-DSC). It was found that Fe₂O₃ and Fe₃O₄ nanoparticles had high catalysis activity on decomposition of AP. The results can be used as a comprehensive experimental course in the instrument analysis laboratroy. The students can learn the hydrothermal method and learn how to use XRD, thermal analysis and other means to characterize the compounds.
- Fe₂O₃ nanoparticles,
- Fe₃O₄ nanoparticles,
- Ammonium perchlorate,
- Thermal analysis,
- Catalysis
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Preparation of Fe₂O₃ and Fe₃O₄ Nanoparticles and the Catalytic Performance for Thermal Decomposition of Ammonium Perchlorate