Citation: ZHANG Xi, LIU Weilun, LU Ya'nan, LÜ Yunkai. Recent advances in the application of headspace gas chromatography-mass spectrometry[J]. Chinese Journal of Chromatography, ;2018, 36(10): 962-971. doi: 10.3724/SP.J.1123.2018.05013 shu

Recent advances in the application of headspace gas chromatography-mass spectrometry

ZHANG Xi ^1, ,
LIU Weilun ¹ ,
LU Ya'nan ² ,
LÜ Yunkai ¹

1.
Key Laboratory of Analytical Science and Technology of Hebei Province, College of Chemistry and Environmental Science, Hebei University, Baoding 071002, China;
2.
Hebei Research Institution for Product Quality Supervision and Inspection, Shijiazhuang 050091, China

Received Date: 12 May 2018

Fund Project: National Natural Science Foundation of China (No. 21375032)

As a sample preparation technique without extraction by organic solvent, headspace analysis is usually combined with gas chromatography-mass spectrometry (GC-MS) to analyze volatile organic compounds in complex matrices. Headspace gas chromatography-mass spectrometry (HS-GC-MS) is a fast, efficient, green, and sensitive technique, and thus it plays an important role in routine analysis. A brief overview of static headspace, dynamic headspace, headspace solid-phase microextraction and GC-MS is provided, followed by the impact of the analysis system and the optimization process. According to the matrix type classification, the application of HS-GC-MS in the analysis of food samples, environment samples, biology samples, etc. is reviewed. This report clearly indicates that the ongoing research on HS-GC-MS is active and new applications are emerging. It has significant prospects for the analysis of volatile organic compounds.
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