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Citation: YU Qiongwei, FANG Kaimin, HE Xiaomei, ZHENG Jie, FENG Yuqi. Preparation of zirconia nanoparticles deposited cotton fibers and their application in the rapid enrichment of phosphopeptides[J]. Chinese Journal of Chromatography, ;2018, 36(3): 237-244. doi: 10.3724/SP.J.1123.2017.11055 shu

Preparation of zirconia nanoparticles deposited cotton fibers and their application in the rapid enrichment of phosphopeptides

Key Laboratory of Analytical Chemistry for Biology and Medicine(Ministry of Education), College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, China

Received Date: 30 November 2017

Fund Project: National Natural Science Foundation of China (Nos. 31671929, 31670373).

A kind of cotton-based fibrous adsorbent, zirconia nanoparticles coated cotton fiber (ZrO₂-CF), was successfully prepared by liquid-phase deposition of zirconia nanoparticles on the surface of cotton fiber. And the ZrO₂-CF fibrous adsorbent was packed in pipet tips for the enrichment of phosphopeptide by pipetting up and down within 2 min, which was simple and fast. Nine phosphopeptides were identified from the digestion of β-casein after ZrO₂-CF extraction. ZrO₂-CF exhibited good selectivity in the enrichment of phosphopeptides from the digestion mixture of β-casein and BSA (molar ratio is 1:100) in which four phosphopeptides were identified. And it also showed excellent extraction efficiency in actual biological samples such as non-fat milk and human serum in which four and nine phosphopeptides were identified, respectively.
- zirconia,
- nanoparticles,
- liquid phase deposition,
- phosphopeptide,
- enrichment
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