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Citation: ZHANG Baile, GAO Lihong, XIE Yingshuang, ZHOU Wei, CHEN Xiaofeng, LEI Chunni, ZHANG Huan. Rapid screening the alkaloids of poppy shell in hot pot condiment, beef noodle soup and seasoning by direct analysis in real time-tandem mass spectrometry[J]. Chinese Journal of Chromatography, ;2017, 35(7): 724-729. doi: 10.3724/SP.J.1123.2017.03022 shu

Rapid screening the alkaloids of poppy shell in hot pot condiment, beef noodle soup and seasoning by direct analysis in real time-tandem mass spectrometry

1.
College of Geography and Environment Science, Northwest Normal University, Lanzhou 730070, China;
2.
Central Laboratory of Technical Center, Gansu Entry-Exit Inspection and Quarantine Bureau, Lanzhou 730010, China

Received Date: 20 March 2017

A direct analysis in real time tandem mass spectrometry (DART-MS/MS) method was established for quickly screening five illegally added alkaloids of poppy shell from the hot pot condiment, beef noodle soup and seasoning. The samples were extracted and purified by acetonitrile, and then injected under the conditions of ionization temperature of 300℃, grid electrode voltage of 150 V and sampling rate of 0.8 mm/s using DART in the positive ion mode. The determination was conducted by tandem mass spectrometry in positive ESI mode under multiple reaction monitoring (MRM) mode. The method is simple and rapid, and can meet the requirement of rapid screening and analysis of large quantities of samples.
- direct analysis of real time-tandem mass spectrometry (DART-MS/MS),
- rapid screening,
- alkaloid of poppy shell,
- illegally added
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1.
沈阳化工大学材料科学与工程学院沈阳 110142

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