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Citation: SUN Yaming, WU Qi, GAO Jie, ZHANG Xia, ZHAO Liang, DONG Shuqing. Determination of cinnamic acid and its derivatives by dispersive solid phase microextraction of graphene quantum dots magnetic composite nanoparticles coupled with capillary electrophoresis[J]. Chinese Journal of Chromatography, ;2017, 35(3): 325-331. doi: 10.3724/SP.J.1123.2016.10017 shu

Determination of cinnamic acid and its derivatives by dispersive solid phase microextraction of graphene quantum dots magnetic composite nanoparticles coupled with capillary electrophoresis

SUN Yaming ^1,2, ,
WU Qi ^1,2 ,
GAO Jie ^1,2 ,
ZHANG Xia ¹ ,
ZHAO Liang ¹ ,
DONG Shuqing ¹

1.
Key Laboratory of Chemistry of Northwestern Plant Resources of Chinese Academy of Sciences, Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China;
2.
University of Chinese Academy of Sciences, Beijing 100049, China

Received Date: 9 October 2016

Fund Project: National Natural Science Foundation of China (Nos. 21405161, 21675163).

Composites of graphene quantum dots (GQDs) and Fe₃O₄(Fe₃O₄-GQDs) nanoparticles were prepared via a one-step co-precipitation approach. And the synthesized Fe₃O₄-GQDs nanoparticles were applied to the extraction of five compounds of cinnamic acid and its derivatives (cinnamic acid, 3,4-dimethoxycinnamic acid, 4-methoxycinnamic acid, ferulic acid and trans-4-hydroxycinnamic acid). Cinnamic acid and its derivatives were detected by capillary electrophoresis (CE). The pH of adsorption solution, adsorption time, amount of adsorbent and desorption time were investigated. The rapid and efficient preconcentration of the five cinnamic acid and its derivatives was successfully obtained with the satisfactory recoveries of 86.2%-96.2%, and relative standard deviations of 1.8%-4.3%. The results indicated that Fe₃O₄-GQDs magnetic nanoparticles were good pretreatment alternatives.
- capillary electrophoresis (CE),
- graphene quantum dots (GQDs),
- magnetic nanoparticles,
- ferroferric oxide (Fe₃O₄),
- cinnamic acid and its derivatives
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