Citation: BAI Junying, HUANG Renhua, LU Yunmei, YU You, WANG Dan. Optimization of headspace solid phase micro-extraction combined with gas chromatography-mass spectrometry conditions of volatile flavor from Feijoa sellowiana leaves[J]. Chinese Journal of Chromatography, ;2016, 34(8): 778-782. doi: 10.3724/SP.J.1123.2016.04006 shu

Optimization of headspace solid phase micro-extraction combined with gas chromatography-mass spectrometry conditions of volatile flavor from Feijoa sellowiana leaves

1.
College of Life Science and Engineering, Southwest University of Science and Technology, Mianyang 621010, China

Corresponding author: HUANG Renhua,
Received Date: 5 April 2016

Fund Project:

To establish the appropriate extraction conditions for the analysis of volatile constituents from Feijoa sellowiana leaves by headspace solid phase micro-extraction (HS-SPME) combined with gas chromatography-mass spectrometry (GC-MS), the extraction conditions were investigated by orthogonal tests. The sum of the peak areas and total peak numbers of the volatile constituents were used as indices to optimize the extraction conditions by using L₉(3⁴) orthogonal array design. The results showed that the influence of temperature was larger and that of the sample amount was smaller for total peak numbers and peak areas. The optimum HS-SPME parameters were selected as follows: 0.6 g sample, extracted for 50 min at 50 ℃, and then desorbed for 6 min. Under these conditions, a total of 88 substances were detected. These substances can reflect the fragrant chemical components of Feijoa sellowiana leaves, and provide some references for the development and utilization of the leaves.
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沈阳化工大学材料科学与工程学院沈阳 110142