Citation: GAN Wei, LIU Xuemin, SUN Jing. Regression evaluation index intelligent filter method for quick optimization of chromatographic separation conditions[J]. Chinese Journal of Chromatography, ;2015, 33(2): 140-145. doi: 10.3724/SP.J.1123.2014.09040 shu

Regression evaluation index intelligent filter method for quick optimization of chromatographic separation conditions

GAN Wei ^1,, ,
LIU Xuemin ² ,
SUN Jing ¹

1.
1. Chongqing Environmental Monitoring Center, Chongqing 401147, China;

Corresponding author: GAN Wei,
Received Date: 25 September 2014
Available Online: 10 December 2014

This paper presents a method of regression evaluation index intelligent filter method (REIFM) for quick optimization of chromatographic separation conditions. The hierarchical chromatography response function was used as the chromatography-optimization index. The regression model was established by orthogonal regression design. The chromatography-optimization index was filtered by the intelligent filter program, and the optimization of the separation conditions was obtained. The experimental results showed that the average relative deviation between the experimental values and the predicted values was 0.18% at the optimum and the optimization results were satisfactory.
1. [1]
  [1] Bian K, Lin T, Liu M, et al. Chinese Journal of Chromatography (卞愧, 林涛, 刘敏, 等. 色谱), 2014, 32(2): 162
2. [2]
  [2] Wang D Y, Zhu J B, Ding Y, et al. Chinese Journal of Chromatography (王定颖, 朱靖博, 丁燕, 等. 色谱), 2014, 32(6): 604
3. [3]
  [3] Qiao K L, Lü J. Journal of Yan'an University: Natural Science Edition (乔克林, 吕佳. 延安大学学报: 自然科学版), 2009, 28(2): 34
4. [4]
  [4] Zhu W Y. Application of Orthogonal and Orthogonal Regression Method. Shenyang: Liaoning People's Publishing House (朱伟勇. 正交与回归正交试验法的应用. 沈阳: 辽宁人民出版社), 1978: 84
5. [5]
  [5] Chen J S. Experimental Study on Metallurgical Methods. Beijing: Metallurgical Industry Press (陈建设. 冶金试验研究方法. 北京: 冶金工业出版社), 2005: 65
6. [6]
  [6] Li Z Z. Chinese Journal of Spectroscopy Laboratory (李志洲. 光谱实验室), 2012, 29(5): 3047
7. [7]
  [7] Gu Y Y. Computer Applications and Software (顾运筠. 计算机应用与软件), 2005, 22(1): 137
8. [8]
  [8] Chen G Y, Le A P. Chinese Journal of Health Laboratory Technology (陈国员, 乐爱平. 中国卫生检验杂志), 2010, 20(10): 2518
9. [9]
  [9] Yang L, Chen Y P. Mathematica Numerica Sinica (杨柳, 陈艳萍. 计算数学), 2008, 30(4): 388
10. [10]
  [10] Shi L, Zhang Z W. Journal of Chinese Medicinal Materials (石磊, 张振巍. 中药材), 2011, 34(12): 1946
11. [11]
  [11] Yu Y M, Wang J H, Zhang S Z, et al. Journal of Nanjing Forestry University: Natural Science Edition (于永明, 王军辉, 张宋智, 等. 南京林业大学学报: 自然科学版), 2011, 35(4): 47
12. [12]
  [12] Xiao R F, Liu J Y, Zhang J Q. Technology of Water Treatment (肖入峰, 刘景洋, 张建强. 水处理技术), 2012, 38(6): 49
13. [13]
  [13] Zhan F, Shao J, Han Y P. Food Science (战峰, 邵婧, 韩泳平. 食品科学), 2011, 32(16): 196
14. [14]
  [14] Liu Z Q, Chen Y L. Journal of the Chinese Cereals and Oils Association (刘竹青, 陈有亮. 中国粮油学报), 2013, 28(2): 48
15. [15]
  [15] Dong R, Tang M L, Wu Y X, et al. Xinjiang Agricultural Sciences (董瑞, 唐明磊, 吴玉霞, 等. 新疆农业科学), 2012, 49(4): 646
16. [16]
  [16] Lu M, Tang H R, Yu S J, et al. Journal of Fruit Science (鲁敏, 汤浩茹, 余世杰, 等. 果树学报), 2011, 28(1): 171
17. [17]
  [17] Yang J P, Liu Z G, Li M, et al. Hydrometallurgy of China (阳建平, 柳召刚, 李梅, 等. 湿法冶金), 2013, 32(1): 27
18. [18]
  [18] Zou H F, Zhang Y K, Lu P Z. High Performance Liquid Chromatography. Beijing: Science Press (邹汉法, 张玉奎, 卢佩章. 高效液相色谱法. 北京: 科学出版社), 1998: 210
19. [19]
  [19] Da S L. Introduction to Chromatography. Wuhan: Wuhan University Press (达世禄. 色谱学导论. 武汉: 武汉大学出版社), 1999
20. [20]
  [20] Lu P Z, Zhang Y K, Liang X M. High Performance Liquid Chromatography and Its Expert System. Shenyang: Liaoning Science and Technology Publishing House (卢佩章, 张玉奎, 梁鑫淼. 高效液相色谱法及其专家系统. 沈阳: 辽宁科学技术出版社), 1992: 307
21. [21]
  [21] Li Y Y, Hu C R. Experiment Design and Data Processing. Beijing: Chemical Industry Press (李云雁,胡传荣. 试验设计与数据处理. 北京: 化学工业出版社), 2008: 171
22. [22]
  [22] Yu X J, Ding G S, Jin D L, et al. Journal of Zhejiang Sci-Tech University (俞晓晶, 丁高松, 金达莱, 等. 浙江理工大学学报), 2009, 26(2): 219
23. [23]
  [23] Du Y P. Modern Instrumental Analysis Method. Shanghai: East China University of Science and Technology Press (杜一平. 现代仪器分析方法. 上海: 华东理工大学出版社), 2008: 45
24. [24]
  [24] Liu L M. Southwest University (刘丽敏. 西南大学), 2008
25. [25]
  [25] Snyder L R, Kirkland J J, Glajch J L, ed. Zhang Y K, Wang J, Zhang W B, transl. Practical HPLC Method Development. Beijing: Sino-culture Press (森德尔L R, 柯克兰J J, 格莱吉克J L, 著. 张玉奎, 王杰, 张维冰, 译. 实用高效液相色谱法的建立. 北京: 华文出版社), 2001: 383
26. [26]
  [26] Zhu P L. Analysis and Testing Technology and Instruments (朱彭龄. 分析测试技术与仪器), 2010, 3(1): 56
27. [27]
  [27] Fa Y, Xu X, Lei X L. Chinese Journal of Scientific Instrument (法洋, 许旭, 雷晓玲. 仪器仪表学报), 2005, 26(S1): 181
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