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Citation: KONG Guang-Hui, LI Yong, LIU Ya-Li. Determination of Lead, Cadmiun, Nickel, and Chromiun in Soil by Temperature Programed Digestion-Atomic Absorption Spectrometry[J]. Chinese Journal of Analytical Chemistry, ;2012, 40(12): 1950-1951. doi: 10.3724/SP.J.1096.2012.20890 shu

Determination of Lead, Cadmiun, Nickel, and Chromiun in Soil by Temperature Programed Digestion-Atomic Absorption Spectrometry

1.
Analysis & Test center, Yunnan Academy of Tobacco Agricultural Sciences, Yuxi 653100, China

Corresponding author: KONG Guang-Hui,
Received Date: 3 September 2012
Available Online: 15 October 2012
Fund Project: 本文系云南省烟草专卖局基金(No.2011YN03)资助 (No.2011YN03)

A temperature programed digestion-atomic absorption spectrometry method was established for the determination of lead, cadmiun, nickel, and chromiun in soil. The temperature program for digestion was set as 80℃ for 1 h, 120℃ for 2 h, and 300℃ for the remove of acid solution. The result shows that the average recoveries for lead, cadmiun, nickel, and chromiun were 100.4%, 99.4%, 95.0%, and 94.0%, respectively. Verified by the standard samples GBW07406 and GBW07407, the established method was found to have a good accuracy. In compariaon with the traditional digestion method, the established method in this atudy was proved to have better accuracy and precision. This method was also proved to have good operability and it's easy to spread.
- Temperature programed digestion
1. [1]
  1 HAN Ping, WANG Ji-Hua, LU An-Xiang, MA Zhi-Hong, PAN Li-Gang. Spectroscopy Spectral Analysis, 2012, 13(3):826-829
2. [2]
  韩平, 王纪华, 陆安祥, 马智宏, 潘立刚. 光谱学与光谱分析Jin-Chao. E, 2012, 13(3):826-829
3. [3]
  2 CHEN Chun, LIU Dan, LU Xin-Yan, LI Jin-Feng, WANG Qi, SHEN nvir. Monit. Forew., 2011, 3(2): 16-20
4. [4]
  陈纯, 刘丹, 路新燕, 李金峰, 王琪, 申进朝. 环境监控与预警, 2011, 3(2): 16-20
5. [5]
  3 WANG Lin-Ping, ZHANG Jun, SUN Hai-Xu, MA Jing-Jing, TU Bu-Xin, GUO Wei, YUAN Zhuo-Bin. Chinese J. Anal. Chem., 2009, 37(5): A027
6. [6]
  王林平, 张君, 孙海旭, 马静静, 图布新, 郭伟, 袁倬斌. 分析化学, 2009, 37(5): A027
7. [7]
  4 FAN Qin-Qin, YANG Xu-Ri, WANG Ya-Ping, ZHOU Yong, ZHOU Ying. Chinese J. Anal. Chem., 2009, 37(5): A059
8. [8]
  范琴琴, 杨旭日, 王萍亚, 周勇, 周瑛. 分析化学, 2009, 37(5): A059
9. [9]
  5 LIU Feng-Zhi, CAI Ming, LIU Yan. NY/T1613-2008. Beijing: Standards Press of China, 2008
10. [10]
  刘凤枝, 蔡明, 刘岩. NY/T1613-2008. 北京: 中国标准出版社, 2008
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