Citation: GUO Wei, YAN Rui-Fang, YUAN Jian-Mei, ZHANG Zhu-Jun, MIAO Jiang-Huan. Time-resolved Post-Chemiluminescence Analysis for Simultaneous Determination of Amikacin and Hydrochlorothiazide[J]. Chinese Journal of Analytical Chemistry, ;2012, 40(12): 1907-1912. doi: 10.3724/SP.J.1096.2012.20255 shu

Time-resolved Post-Chemiluminescence Analysis for Simultaneous Determination of Amikacin and Hydrochlorothiazide

1.
¹ Department of Chemistry, Xinxiang Medical University, Xinxiang 453003, China;

Corresponding author: GUO Wei,
Received Date: 13 March 2012
Available Online: 12 August 2012
Fund Project: 本文系国家自然科学基金资助项目(No.30470886) (No.30470886)

Based on the differential chemiluminescent rate of amikacin (AMK) and hydrochlorothiazide (HCT) in the system of Luminol-peroxymonosulfate (PMS), a novel time-resolved post-chemiluminescence method was established for the simultaneous determination of AMK and HCT. The HCT system gives the highest chemiluminescence intensity at 1 s, whereas the AMK system gives its most intense chemiluminescence emission at 39.7 s. The kinetic curve showed two separate chemiluminescence peaks at different time without disturbing each other. Under the optimum conditions described above, the analytical performance was obtained. The linear response for the determination of HCT and AMK was in the range from 8.0×10^-5 to 4.0×10^-3 g/L and from 8.0×10^-4 to 4.0×10^-2 g/L. The relative standard diviation of AMK (4.0×10^-3 g/L) and HCT (4.0×10^-4 g/L) are 3.7% and 2.4% (n=11), and the detection limit (3) of AMK and HCT are 2.0×10^-4 g/L and 2.0×10^-5 g/L, respectively.
- Time-resolved,
- Post-chemiluminescence,
- Peroxymonosulfate,
- Luminol,
- Amikacin,
- Hydrochlorothiazide
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沈阳化工大学材料科学与工程学院沈阳 110142