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Citation: YU Longbao, XU Hu, SHI Yayu, ZHANG Wenpeng, YIN Hengbo, ZHANG Xiongfei. Preparation of NiO Nanoparticles Supported on SBA-15 Mesoporous Molecular Sieve Modified by Schiff Base Monomer[J]. Chinese Journal of Applied Chemistry, ;2013, 30(10): 1163-1168. doi: 10.3724/SP.J.1095.2013.20595 shu

Preparation of NiO Nanoparticles Supported on SBA-15 Mesoporous Molecular Sieve Modified by Schiff Base Monomer

School of Chemistry and Chemical Engineering, Jiangsu Uiniversity, Zhenjiang 212012, China

Received Date: 21 December 2012
Revised Date: 31 January 2013

With copolymeric modification by Schiff base monomer,NiO nanoparticles supported on SBA-15 mesoporous molecular sieves were prepared and characterized by powder X-ray diffraction (XRD),UV-Vis spectrometer,high resolution transmission electron microscopy(HRTEM) and N₂ adsorption-desorption isotherms. The results show that the as-prepared samples possess a bi-dimensional P6mm hexagonal symmetry of the pores and the formed NiO nanoparticles are mainly dispersed into channels of SBA-15. When the loadings of Schiff base monomer are less than 10%,the pore diameter is in the range of 6~8 nm. Increasing the loading of Schiff base monomer up to 15%,the channels of SBA-15 are severely blocked by encapsulated NiO nanoparticles and the pore diameter is reduced to 3.8 nm. In addition,NiO nanoparticle size increases with increasing Schiff base monomer loading.
- mesoporous molecular sieve,
- Schiff base,
- nickle oxide,
- nanoparticle
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