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Citation: MA Youmei, YANG Xiaoping, JIA Xiaolong, GUO Lijuan. A Simple and Controllable Preparation of PbS Nanobelts[J]. Chinese Journal of Applied Chemistry, ;2012, 29(5): 557-564. doi: 10.3724/SP.J.1095.2012.00382 shu

A Simple and Controllable Preparation of PbS Nanobelts

1.
State Key Laboratory of Organic-Inorganic Composites, College of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing 100039, China

Corresponding author: YANG Xiaoping,
Received Date: 30 August 2011
Available Online: 15 October 2011

PbS nanobelts were synthesized by a facile hydrothermal method using lead nitrate,thioacetamide and dodecyl benzene sulfonate(SDBS) as raw materials.SDBS played a dual role as both the starting material and surfactant in the reaction.The as-prepared nanobelts were characterized by transmission electron microscopy and X-ray diffraction.The photoluminescence property of the nanobelts was also studied.It was concluded that the intermediate PbSO₄ could act as a template for the growth of PbS nanobelts under hydrothermal conditions.The formation mechanism of nanobelts was further investigated.The results indicated that the intermediate PbSO₄ could paly restriction effect on the surfactant(SDBS).When PbSO₄ was replaced by other lead composite,the surfactant would lose its role and irregular micro-crystals were obtained consequently.The formation of nanobelts was readily controlled under a slow reaction speed.The result presented here may open an efficient way to synthesizing nanobelts with different morphologies.
- micro-crystals,
- template effect,
- morphology control,
- lead sulfide nanobelts
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