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Citation: ZHAO Xinmei, QIU Fubao, WANG Haishui. Influence of Mn²⁺ on the Morphological Control of ZnS Nanoparticles[J]. Chinese Journal of Applied Chemistry, ;2012, 29(2): 191-195. doi: 10.3724/SP.J.1095.2012.00154 shu

Influence of Mn²⁺ on the Morphological Control of ZnS Nanoparticles

1.
a Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China;
2.
b School of Chemistry & Chemical Engineering, South China University of Technology, Guangzhou 510640, China

Corresponding author: WANG Haishui,
Received Date: 15 April 2011
Available Online: 3 June 2011
Fund Project: 国家自然科学基金(20873136)资助项目 (20873136)

ZnS nanoparticles on the self-assembled monolayer of 3-sulfopropyltrimethoxylsilane were fabricated by the reaction between ZnSO₄ and thioacetamide in aqueous solution.It was found that a compact ZnS nanoparticle film with string-like particles was obtained when the aqueous solution contained only Zn²⁺.Interestingly,the morphology of ZnS nanoparticles changed from the compact film to hemispheres with herringbone-like structure when Mn²⁺ was added into the aqueous solution.XRD and EDS results indicated that the manganese ions were not doped into the ZnS nanoparticles.These experimental results showed that Mn²⁺ played a key role in the morphological control of the ZnS nanoparticles,even though Mn²⁺ ions were absent in the final as-prepared products.The mechanism of the formation of ZnS with Mn²⁺ presence was discussed.
- ZnS,
- nanoparticles,
- morphology control,
- manganese ions
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Influence of Mn²⁺ on the Morphological Control of ZnS Nanoparticles