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Citation: SONG Hong, MAO Huiyu, SHI Deqing. Synthesis and Herbicidal Activity of N-[2-(4,6-Dimethoxypyrimidin-2-yloxy) benzylidene]-2-aryloxyacetohydrazides[J]. Chinese Journal of Applied Chemistry, ;2011, 28(10): 1173-1178. doi: 10.3724/SP.J.1095.2011.00633 shu

Synthesis and Herbicidal Activity of N-[2-(4,6-Dimethoxypyrimidin-2-yloxy) benzylidene]-2-aryloxyacetohydrazides

SONG Hong ^a,b ,
MAO Huiyu ^a,b ,
SHI Deqing ^a,,

1.
a Key Laboratory of Pesticide and Chemical Biology of Ministry of Education, College of Chemistry, Central China Normal University, Wuhan 430079;
2.
b Wuhan Bioengineering Institute, Yangluo District, Wuhan

Corresponding author: SHI Deqing,
Received Date: 25 October 2010
Available Online: 13 January 2011
Fund Project: 国家自然科学基金(20872046) (20872046)湖北省自然科学基金(2008CDB086)资助项目 (2008CDB086)

A series of novel N-[2-(4,6-dimethoxypyrimidin-2-yloxy) benzylidene]-2-aryloxyacetohydrazides 3 was synthesized by the condensation reactions of 2-(4,6-dimethoxypyrimidin-2-yloxy) benzaldehyde 1 with various 2-aryloxyacetohydrazides 2.Their structures were characterized by IR,¹H NMR,EI-MS,ESI-MS and elemental analysis.The results of bioassay(in vivo) indicated that most of the title compounds 3 possessed good herbicidal activities against Amaranthus retroflexus in both pre-emergence and post-emergence treatments at the dose of 1.5 kg/hm².
- pyrimidinyl carboxylic acid,
- aryloxyacetohydrazide,
- herbicidal activity
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