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Citation: SUN Haojian, MA Yiwen, WANG Yuanrui, ZHANG Long. New Synthetic Process of Dicyclopentadiene Phenol Resin[J]. Chinese Journal of Applied Chemistry, ;2011, 28(6): 629-633. doi: 10.3724/SP.J.1095.2011.00469 shu

New Synthetic Process of Dicyclopentadiene Phenol Resin

1.
Jilin Provincial Engineering Laboratory for the Complex Utilization of Biomass and Petroresources, School of Chemical Engineering, Changchun University of Technology, Changchun 130012

Corresponding author: ZHANG Long,
Received Date: 9 August 2010
Available Online: 6 November 2010
Fund Project: 吉林省科技发展计划项目(20070509) (20070509)

Dicyclopentadiene phenol resin(DPR) was prepared from dicyclopentadiene and phenol with methane sulfonic acid as the catalyst.The optimum conditions for the synthesis were as follows:n(phenol)/n(DCPD)=5;w(catalyst)=1.5%;temperature=120℃;time=5 h;yield=89%.The light yellow dicyclopentadiene phenol resin was obtained by the decolouring of catalytic-hydrogenation.The optimal conditions for the decolorization were as follows:hydrogen pressure=1.5 MPa,w(Pd/Al₂O₃)=0.5%,temperature=80℃,yield=89%.FT-IR and ¹H NMR analysis identified the desired product.The product properties reached the international quality standards.
- dicyclopentadiene,
- phenol,
- decolorization,
- dicyclopentadiene phenol resin
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