Citation: FANG Lan-Yun,  JIANG Yan-Hua,  LI Ji-Ge,  QIU Qiao-Li,  JIN Mi-Cong,  ZHANG Dan-Dan,  ZHANG Yu-Mei. Determination of Bongkrekic Acid in Food by Dispersive Solid Phase Extraction-High Performance Liquid Chromatography-Tandem Mass Spectrometry Using Nitro Modified Zirconium Metal Organic Framework[J]. Chinese Journal of Analytical Chemistry, ;2023, 51(6): 1024-1032. doi: 10.19756/j.issn.0253-3820.231040 shu

Determination of Bongkrekic Acid in Food by Dispersive Solid Phase Extraction-High Performance Liquid Chromatography-Tandem Mass Spectrometry Using Nitro Modified Zirconium Metal Organic Framework

  • Corresponding author: ZHANG Yu-Mei, 23858956@qq.com
  • Received Date: 10 February 2023
    Revised Date: 7 April 2023

    Fund Project: Supported by the Basic Public Welfare Research Project of Zhejiang Province (No. LGC22H260002), the Ningbo Public Welfare Key Project (No. 2022S091) and the Ningxia Natural Science Foundation (No. 2022AAC03208).

  • Dispersive solid phase extraction (DSPE) using nitro modified zirconium-based metal organic framework (NO2-MOF) as adsorbent for determination of bongkrekic acid in food was developed. The synthesized NO2-MOF were characterized by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), infrared spectroscopy (IR), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and nitrogen adsorption experiment, etc, indicating that a structural stable MOF material with large BET surface area was obtained. There existed electrostatic interaction, π-π stacking, hydrogen bond and other weak intermolecular interactions between MOF and bongkrekic acid molecules to achieve selective adsorption of target molecules. Main experimental factors affecting DSPE were optimized, including pH value, amount of the adsorbent, extraction time, and type of desorption solvent. The established method was applied to detection of bongkrekic acid in auricularia auricula and rice flour, with limit of quantification of 1.6 μg/kg, and limit of detection of 0.5 μg/kg. In conclusion, the established method for determination of bongkrekic acid in food by DSPE had the advantages such as short pretreatment time, high sensitivity and precision with satisfactory recoveries of 75%-96%, and was environmentally friendly. This work provided a more reliable technique for determination of extremely trace amount of bongkrekic acid in related food such as auricularia auricula, tremella and rice flour.
  • 加载中
    1. [1]

      MOEBIUS N, ROSS C, SCHERLACH K, ROHM B, ROTH M, HERTWECK C. Chem. Biol., 2012, 19(9):1164-1174.

    2. [2]

      MATSUMOTO K, SUYAMA M, FUJITA S, MORIWAKI T, SATO Y, ASO Y, MUROSHITA S, MATSUO H, MONDA K, OKUDA K, ABE M, FUKUNAGA H, KANO A, SHINDO M. Chem. Eur. J., 2015, 21(32):11590-11602.

    3. [3]

    4. [4]

    5. [5]

    6. [6]

    7. [7]

    8. [8]

    9. [9]

    10. [10]

      MAYA F, CABELLO C P, FRIZZARIN R M, ESTELA J M, PALOMINO G T, CERDA V. TrAC, Trends Anal. Chem., 2017, 90:142-152.

    11. [11]

      LIAN L, ZHANG X, HAO J, LV J, WANG X, ZHU B, LOU D J. J. Chromatogr. A, 2018, 1579:1-8.

    12. [12]

      RAHMAN M M, ABD EL-ATY A M, KIM S W, SHIN S C, SHIN H C, SHIM J H. J. Sep. Sci., 2017, 40(1):203-212.

    13. [13]

      CASTILLO-GARCÍA M L, AGUILAR-CABALLOS M P, GOMEZ-HENS A. TrAC, Trends Anal. Chem., 2016, 82:385- 393.

    14. [14]

      KHEZELI T, DANESHFAR A. TrAC, Trends Anal. Chem., 2017, 89:99-118.

    15. [15]

      RÍOS A, ZOUGAGH M. TrAC, Trends Anal. Chem., 2016, 84:72-83.

    16. [16]

      SOCAS-RODRÍGUEZ B, HERRERA-HERRERA A V, ASENSIO-RAMOS M, HERNÁNDEZ-BORGES J. J. Chromatogr. A, 2014, 1357:110-146.

    17. [17]

      DE TOFFOLI A L, MACIEL E V S, FUMES B H, LANÇAS F M. J. Sep. Sci., 2018, 41(1):288-302.

    18. [18]

      RUIZ F J, RIPOLL L, HIDALGO M, CANALS A. Talanta, 2019, 191:162-170.

    19. [19]

      ZHANG H, XIONG P, LI G. TrAC, Trends Anal. Chem., 2020, 131:116015.

    20. [20]

    21. [21]

      DOU Y, GUO L, LI G, LV X, XIA L, YOU J. Microchem. J., 2019, 146:366-373.

    22. [22]

      RADA Z H, ABID H R, SUN H, SHANG J, LI J, HE Y, LIU S, WANG S. Prog. Nat. Sci.:Mater. Int., 2018, 28(2):160- 167.

    23. [23]

      HIRA S A, NAGAPPAN S, ANNAS D, KUMAR Y A, PARK K H. Electrochem. Commun., 2021, 125:107012.

    24. [24]

      GARIBAY S J, COHEN S M. Chem. Commun., 2010, 46(41):7700-7702.

    25. [25]

      LU D, LIU C, QIN M, DENG J, SHI G, ZHOU T. Anal. Chim. Acta, 2020, 1133:88-98.

  • 加载中
    1. [1]

      Yanhui Zhong Ran Wang Zian Lin . Analysis of Halogenated Quinone Compounds in Environmental Water by Dispersive Solid-Phase Extraction with Liquid Chromatography-Triple Quadrupole Mass Spectrometry. University Chemistry, 2024, 39(11): 296-303. doi: 10.12461/PKU.DXHX202402017

    2. [2]

      Wenxiu Yang Jinfeng Zhang Quanlong Xu Yun Yang Lijie Zhang . Bimetallic AuCu Alloy Decorated Covalent Organic Frameworks for Efficient Photocatalytic Hydrogen Production. Acta Physico-Chimica Sinica, 2024, 40(10): 2312014-. doi: 10.3866/PKU.WHXB202312014

    3. [3]

      Zunxiang Zeng Yuling Hu Yufei Hu Hua Xiao . Analysis of Plant Essential Oils by Supercritical CO2Extraction with Gas Chromatography-Mass Spectrometry: An Instrumental Analysis Comprehensive Experiment Teaching Reform. University Chemistry, 2024, 39(3): 274-282. doi: 10.3866/PKU.DXHX202309069

    4. [4]

      Shengbiao Zheng Liang Li Nini Zhang Ruimin Bao Ruizhang Hu Jing Tang . Metal-Organic Framework-Derived Materials Modified Electrode for Electrochemical Sensing of Tert-Butylhydroquinone: A Recommended Comprehensive Chemistry Experiment for Translating Research Results. University Chemistry, 2024, 39(7): 345-353. doi: 10.3866/PKU.DXHX202310096

    5. [5]

      Fugui XIDu LIZhourui YANHui WANGJunyu XIANGZhiyun DONG . Functionalized zirconium metal-organic frameworks for the removal of tetracycline from water. Chinese Journal of Inorganic Chemistry, 2025, 41(4): 683-694. doi: 10.11862/CJIC.20240291

    6. [6]

      Lu XUChengyu ZHANGWenjuan JIHaiying YANGYunlong FU . Zinc metal-organic framework with high-density free carboxyl oxygen functionalized pore walls for targeted electrochemical sensing of paracetamol. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 907-918. doi: 10.11862/CJIC.20230431

    7. [7]

      Bin HEHao ZHANGLin XUYanghe LIUFeifan LANGJiandong PANG . Recent progress in multicomponent zirconium?based metal-organic frameworks. Chinese Journal of Inorganic Chemistry, 2024, 40(11): 2041-2062. doi: 10.11862/CJIC.20240161

    8. [8]

      Simin Fang Hong Wu Sizhe Sheng Lingling Li Yuxi Wang Hongchun Li Jun Jiang . The Food Kingdom Lecture Series: The Science behind Color. University Chemistry, 2024, 39(9): 177-182. doi: 10.12461/PKU.DXHX202402012

    9. [9]

      Hong CAIJiewen WUJingyun LILixian CHENSiqi XIAODan LI . Synthesis of a zinc-cobalt bimetallic adenine metal-organic framework for the recognition of sulfur-containing amino acids. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 114-122. doi: 10.11862/CJIC.20240382

    10. [10]

      Wenjie SHIFan LUMengwei CHENJin WANGYingfeng HAN . Synthesis and host-guest properties of imidazolium-functionalized zirconium metal-organic cage. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 105-113. doi: 10.11862/CJIC.20240360

    11. [11]

      Yikai Wang Xiaolin Jiang Haoming Song Nan Wei Yifan Wang Xinjun Xu Cuihong Li Hao Lu Yahui Liu Zhishan Bo . 氰基修饰的苝二酰亚胺衍生物作为膜厚不敏感型阴极界面材料用于高效有机太阳能电池. Acta Physico-Chimica Sinica, 2025, 41(3): 2406007-. doi: 10.3866/PKU.WHXB202406007

    12. [12]

      Mingyang Men Jinghua Wu Gaozhan Liu Jing Zhang Nini Zhang Xiayin Yao . 液相法制备硫化物固体电解质及其在全固态锂电池中的应用. Acta Physico-Chimica Sinica, 2025, 41(1): 2309019-. doi: 10.3866/PKU.WHXB202309019

    13. [13]

      Xiaofang DONGYue YANGShen WANGXiaofang HAOYuxia WANGPeng CHENG . Research progress of conductive metal-organic frameworks. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 14-34. doi: 10.11862/CJIC.20240388

    14. [14]

      Fan Wu Wenchang Tian Jin Liu Qiuting Zhang YanHui Zhong Zian Lin . Core-Shell Structured Covalent Organic Framework-Coated Silica Microspheres as Mixed-Mode Stationary Phase for High Performance Liquid Chromatography. University Chemistry, 2024, 39(11): 319-326. doi: 10.12461/PKU.DXHX202403031

    15. [15]

      Chongjing Liu Yujian Xia Pengjun Zhang Shiqiang Wei Dengfeng Cao Beibei Sheng Yongheng Chu Shuangming Chen Li Song Xiaosong Liu . Understanding Solid-Gas and Solid-Liquid Interfaces through Near Ambient Pressure X-Ray Photoelectron Spectroscopy. Acta Physico-Chimica Sinica, 2025, 41(2): 100013-. doi: 10.3866/PKU.WHXB202309036

    16. [16]

      Yi DINGPeiyu LIAOJianhua JIAMingliang TONG . Structure and photoluminescence modulation of silver(Ⅰ)-tetra(pyridin-4-yl)ethene metal-organic frameworks by substituted benzoates. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 141-148. doi: 10.11862/CJIC.20240393

    17. [17]

      Tiantian MASumei LIChengyu ZHANGLu XUYiyan BAIYunlong FUWenjuan JIHaiying YANG . Methyl-functionalized Cd-based metal-organic framework for highly sensitive electrochemical sensing of dopamine. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 725-735. doi: 10.11862/CJIC.20230351

    18. [18]

      Yanan Liu Yufei He Dianqing Li . Preparation of Highly Dispersed LDHs-based Catalysts and Testing of Nitro Compound Reduction Performance: A Comprehensive Chemical Experiment for Research Transformation. University Chemistry, 2024, 39(8): 306-313. doi: 10.3866/PKU.DXHX202401081

    19. [19]

      Jing SUBingrong LIYiyan BAIWenjuan JIHaiying YANGZhefeng Fan . Highly sensitive electrochemical dopamine sensor based on a highly stable In-based metal-organic framework with amino-enriched pores. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1337-1346. doi: 10.11862/CJIC.20230414

    20. [20]

      Zelong LIANGShijia QINPengfei GUOHang XUBin ZHAO . Synthesis and electrocatalytic CO2 reduction performance of metal-organic framework catalysts loaded with silver particles. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 165-173. doi: 10.11862/CJIC.20240409

Metrics
  • PDF Downloads(14)
  • Abstract views(1902)
  • HTML views(86)

通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Address:Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888
Powered By info@rhhz.net

/

DownLoad:  Full-Size Img  PowerPoint
Return