Citation: XU Jing, ZHENG Hong, XIE Li-Fang, LIN Wei-Qi, GAO Jing, XIE Ze-Zhong, CHEN Hong-Ju, ZENG Yong-Ming, LIU Guo-Kun, TIAN Zhong-Qun. Fast Detection of Trace Enrofloxacin and Ciprofloxacin in Chicken Meat by Surface-enhanced Raman Spectroscopy[J]. Chinese Journal of Analytical Chemistry, ;2023, 51(3): 397-404. doi: 10.19756/j.issn.0253-3820.221227 shu

Fast Detection of Trace Enrofloxacin and Ciprofloxacin in Chicken Meat by Surface-enhanced Raman Spectroscopy

1.
State Key Laboratory of Marine Environmental Science, College of the Environment and Ecology, Xiamen University, Xiamen 361102, China;
2.
State Key Laboratory of Physical Chemistry of Solid Surface, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005, China;
3.
Market and Quality Supervision Commission of Xiamen Municipality, Xiamen 361000, China;
4.
Xiamen Perser Nano Technology Co. Ltd., Xiamen 361000, China

Corresponding author: LIU Guo-Kun, guokunliu@xmu.edu.cn
Received Date: 9 May 2022
Revised Date: 14 October 2022

Fund Project: Supported by the National Natural Science Foundation of China (No. 41876099), the National Key Research & Development Program of China (No. 2018YFC1602600) and the Xiamen Science and Technology Project (No. 3502Z20183002).

With the increasing public concern on food quality, especially the zero-tolerance of illegal additives, the rapid qualitative and quantitative analysis of trace banned substances in food is in a prosperity stage in the field of food safety. Here, by combining with a self-developed rapid pretreatment kit, an on-site, rapid and sensitive detection strategy for trace antibiotics such as enrofloxacin and ciprofloxacin, two typical abused antibiotics in livestock and other industries, by surface-enhanced Raman spectroscopy (SERS) technique was developed. The abused quinolones residues in chicken meat (3 kinds of silky chicken meat and 2 kinds of plain chicken meat) were successfully screened by the developed SERS method, which showed an accurate qualification and a reliable quantitation in comparison with that by standard high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) technique. The proposed SERS-based strategy may provide a practical and simple method for rapid detection of other quinolones in real samples.
- Quinolone antibiotics,
- Chicken sample,
- Surface-enhanced Raman spectroscopy,
- Detection method
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