Citation: LIANG Wei-Xin, PAN Jia-Chuan, LIN Chen, GUO Peng-Ran. Thermal Extraction-emulsion Injection Combining Single Particle-inductively Coupled Plasma-mass Spectrometry for Determination of Sliver Nanoparticles in Food Packaging[J]. Chinese Journal of Analytical Chemistry, ;2021, 49(9): 1572-1579. doi: 10.19756/j.issn.0253-3820.210463 shu

Thermal Extraction-emulsion Injection Combining Single Particle-inductively Coupled Plasma-mass Spectrometry for Determination of Sliver Nanoparticles in Food Packaging

Guangdong Provincial Key Laboratory of Emergency Test for Dangerous Chemicals, Institute of Analysis, Guangdong Academy of Sciences(China National Analytical Center, Guangzhou), Guangzhou 510070, China

Corresponding author: GUO Peng-Ran, prguo@fenxi.com.cn
Received Date: 25 April 2021
Revised Date: 21 June 2021

Fund Project: Supported by the Key Research Fields Program of Guangdong Province, China (No.2019B020211001) and the Self-financing Projects of Scientific Research of Institute of Analysis, Guangdong Academy of Sciences, China(No.202005).

A method for determination of silver nanoparticles (AgNPs) in antibacterial composite food packaging by thermal extraction-emulsion injection combining single particle-inductively coupled plasma-mass spectrometry (SP-ICP-MS) was developed. The AgNPs were extracted by breaking polyethylene polymer chain using decalin under the conditions of high temperature, and the size distribution, mass and particle concentration of AgNPs were measured by SP-ICP-MS. The method was assessed to obtain the optimal extraction temperature, efficiency and limit of detection, and eventually applied to the determination of actual sample. The results indicated that, the size distribution and particle concentration would not be affected by thermal extraction process, the optimal extraction temperature of two types of antibacterial composite food packaging (film and bags) was 150℃, and the extraction efficiencies were 94.3% and 90.3%, respectively. The limit of detection for particle size was 23 nm. The detection results of actual sample showed the AgNPs contents in 4 types of antibacterial composite food packaging materials were 0.038-4.884 μg/g, the AgNPs ratio and mean size were 0.69%-3.80% and 35.5-85.1 nm, respectively. The proposed method was accurate and rapid for determination of AgNPs in food packaging materials.
- Food packaging material,
- Sliver nanoparticles,
- Decalin,
- Single particle-inductively coupled plasma-mass spectrometry
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