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Citation: Min-Min LIU, Na-Ting HE, Hong-Xu GUO, Shao-Ming YING, Zhang-Xu CHEN. Microwave Pyrolysis and Electrochemical Supercapacitor of S-doped g-C3N4 Nanoparticles[J]. Chinese Journal of Structural Chemistry, ;2021, 40(6): 806-810. doi: 10.14102/j.cnki.0254–5861.2011–3016 shu

Microwave Pyrolysis and Electrochemical Supercapacitor of S-doped g-C3N4 Nanoparticles

  • a.

    College of Chemistry, Chemical Engineering and Environment, Minnan Normal University, Zhangzhou, Fujian 363000, China

  • b.

    Fujian Provincial Key Laboratory of Featured Materials in Biochemical Industry, Ningde Normal University, Ningde, Fujian 352100, China

  • c.

    Fujian Provincial Key Laboratory of Ecology-Toxicological Effects & Control for Emerging Contaminants, Putian University, Putian, Fujian 351100, China

  • Corresponding author: Hong-Xu GUO, guohx@mnnu.edu.cn
  • Received Date: 29 October 2020
    Accepted Date: 21 December 2020

    Fund Project: the Natural Science Foundation of Fujian Province 2020J01803Fujian Provincial Key Laboratory of Featured Materials in Biochemical Industry FJKL_FBCM202004the Fujian Provincial Key Laboratory of Ecotoxicological Effects and Control of New pollutants PY19001

Figures(5)

  • In this study, S-doped g-C3N4 nanoparticles were successfully prepared by one-step solid-state microwave synthesis. The detailed characterizations through XRD, FT-IR, SEM and XPS were studied. In addition, the electrochemical properties as supercapacitor of the sample were tested by cyclic voltammetry (CV), galvanostatic charge-discharge (GCD) and electrochemical impedance spectroscopy (EIS) techniques. The results showed a high specific capacitance of 691 F/g at current density of 4 A/g in 2 M KOH + 0.15 M K3[Fe(CN)6] electrolyte. This study shows that the microwave synthesis is a promising way to design carbon-based electrodes for supercapacitor.
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