Citation: Man-Sheng CHEN, Yi-Fang DENG, Chun-Hua ZHANG, Liang-Bing SHENG, Wei-Hong LU, Jun-Bin SUN. Solvothermal Synthesis, Crystal Structure and Property of a Three-dimensional Fe(II) Complex: [Fe(INAIP)(DMF)]n·0.5nDMF[J]. Chinese Journal of Structural Chemistry, ;2021, 40(5): 625-630. doi: 10.14102/j.cnki.0254–5861.2011–2976 shu

Solvothermal Synthesis, Crystal Structure and Property of a Three-dimensional Fe(II) Complex: [Fe(INAIP)(DMF)]n·0.5nDMF

  • Corresponding author: Man-Sheng CHEN, cmsniu@163.com
  • Received Date: 3 September 2020
    Accepted Date: 4 November 2020

    Fund Project: the Natural Science Foundation of Hunan Province 2020JJ4148the Scientific Research Fund of Hunan Provincial Education Department 18A328the Foundation of Key Laboratory of Functional Organometallic Materials, University of Hunan Province GN19K03the Center for the Functionalization of Metal-organic Frameworks Materials Studies KYJG1802

Figures(5)

  • A Fe-based metal-organic framework, [Fe(INAIP)(DMF)]n·0.5nDMF (1), has been synthesized by the reaction of 5-(isonicotinamido)isophthalic acid (H2INAIP) with FeSO4∙7H2O under DMF reaction solvent. Single-crystal X-ray diffraction analysis indicates that complex 1 displays a two-fold interpenetrated three-dimensional (3D) framework with sra topology. The TG, magnetic and adsorption properties of the complex were also studied.
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