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Citation: Yao-Ming YU, Jia-Jie LIU, Rui QI, Chang-Jian ZUO, Wen-Guang ZHAO, Jun-Liang LU, Ming-Jian ZHANG, Feng PAN. Interface-reconstruction Forming Bifunctional (LixTM1-x)O Rock-salt Shell for Enhanced Cyclability in Li-rich Layered Oxide[J]. Chinese Journal of Structural Chemistry, ;2020, 39(8): 1363-1371. doi: 10.14102/j.cnki.0254–5861.2011–2920 shu

Interface-reconstruction Forming Bifunctional (LixTM1-x)O Rock-salt Shell for Enhanced Cyclability in Li-rich Layered Oxide

  • a.

    School of Advanced Materials, Peking University Shenzhen Graduate School, Shenzhen 518055, China

  • b.

    Center for Advanced Radiation Source (ChemMatCARS), the University of Chicago, Argonne, Illinois 60439, United States

  • Corresponding author: Ming-Jian ZHANG, zhangmj@pkusz.edu.cn Feng PAN, panfeng@pkusz.edu.cn
  • Received Date: 28 June 2020
    Accepted Date: 13 July 2020

    Fund Project: National Key R & D Program of China 2016YFB0700600Soft Science Research Project of Guangdong Province 2017B030301013Shenzhen Science and Technology Research Grant ZDSYS201707281026184

Figures(5)

  • Poor cycling stability, as a long-standing issue, has greatly hindered the commercial application of Li-rich layered oxide cathodes in high-energy-density Li-ion batteries. NiO-type rock-salt phase is commonly considered electrochemically inert but stable. Herein, an ultrathin (LixTM1-x)O rock-salt shell was in situ constructed at the particle surface during the synthesis of Li-rich layered oxide cathodes through a unique soft chemical quenching method. Comprehensive structural/chemical analysis reveals that, it not only inherits the chemical stability of traditional NiO-type rock-salt phase, but also facilitates Li+ diffusion due to the co-occupancy of Li+ and TM cations. Such a bifunctional shell could efficiently prevent TM dissolution and oxygen evolution during the long-term cycling, eventually leading to the enhanced cycling stability for Li-rich layered oxides (92.7% of capacity retention after 200 cycles at 0.5C). It provides new guidance to design and synthesize new Li-rich layered oxides with the excellent cycling stability through utilizing some electrochemically-inert phases.
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