Citation: MA Fa-Xue, ZHAO Dan, ZHANG Rong-Hua, LI Fei-Fei, ZHANG Ai-Yun. A New Coordination Polymer Pb(C12H6O4): Structure Resolution of Non-merohedral Twinning Crystal[J]. Chinese Journal of Structural Chemistry, ;2016, 35(3): 437-441. doi: 10.14102/j.cnki.0254-5861.2011-0846
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Hydrothermal reaction of naphthalene-1, 8-dicarboxylate with PbCl2 leads to a new coordination polymer compound, Pb(C12H6O4). Single-crystal X-ray diffraction analysis reveals that it crystallizes in monoclinic, space group P21/c with a = 13.1648(18), b = 5.3881(8), c = 14.599(2) Å, β = 95.759(2)°, V = 1030.3(3) Å3, Z = 4, Mr = 384.32, Dc = 2.7167 g/cm3, F(000) = 768, μ(MoKα) = 16.37 mm-1, R = 0.043 and wR = 0.097. The structure of Pb(C12H6O4) was refined by two components non-merohedral twinning model with the twin law of (-1000-100.22401) and twinning ratio of 0.736:0.264. In this structure, the Pb atoms are surrounded by five O atoms from ligands into PbO5 polyhedra, which are further interconnected to form a 2D layer structure parallel to the bc-plane.
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