Citation: PAN Ya-Ru, SUN Ming, LI Xiu-Mei. Hydrothermal Syntheses and Crystal Structures of Two Complexes of Cobalt and Manganese Assembled by 4,4'-Oxydibenzoic Acid[J]. Chinese Journal of Structural Chemistry, ;2015, 34(4): 576-584. doi: 10.14102/j.cnki.0254-5861.2011-0566 shu

Hydrothermal Syntheses and Crystal Structures of Two Complexes of Cobalt and Manganese Assembled by 4,4'-Oxydibenzoic Acid

a.
a. Faculty of Chemistry, Tonghua Normal University, Tonghua 134002, China;
b.
b. College of Plant Science, Jilin Agriculture Science and Technology College, Jilin 132101, China

Received Date: 12 November 2014
Available Online: 28 December 2014
Fund Project: the Science and Technology Research Projects of the Education Office of Jilin Province (No. 2013. 384) (201205080)

Two new coordination polymers [Co(oba)(mbix)]_2n·nH₂O (1) and [Mn(Hoba)2(H₂O)₂]_n (2) (H₂oba=4,4'-oxydibenzoic acid, mbix=1,3-bis(imidazol-1-ylmethyl)benzene) have been successfully synthesized under hydrothermal conditions. Their structures have been determined by elemental analyses, IR spectroscopy, UV and single-crystal X-ray diffraction analysis. The intermolecular hydrogen bonding and π-π stacking interactions extend the complexes into a 3D supramolecular structure.
- hydrothermal synthesis,
- crystal structure,
- Co(Ⅱ) complex,
- Mn(Ⅱ) complex
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