Citation: WANG Zhumei, LI Yueming, WAN Detian, ZUO Jianlin, SHEN Zongyang, LI Kai. Preparation and Stability of Silica Coated Bismuth-Based Yellow Pigments[J]. Chinese Journal of Applied Chemistry, ;2020, 37(1): 109-116. doi: 10.11944/j.issn.1000-0518.2020.01.190200 shu

Preparation and Stability of Silica Coated Bismuth-Based Yellow Pigments

WANG Zhumei ^a ,
LI Yueming ^a,, ,
WAN Detian ^a,b,, ,
ZUO Jianlin ^a ,
SHEN Zongyang ^a ,
LI Kai ^a

a.
School of Materials Science and Engineering, Jingdezhen Ceramic Institute, Jingdezhen, Jiangxi 333001, China
b.
State Key Laboratory of Green Building Materials, China Building Materials Academy, Beijing 100024, China

Corresponding author: LI Yueming, lym6329@163.com; dtwan@ctc.ac.cn WAN Detian, dtwan@ctc.ac.cn
Received Date: 17 July 2019
Revised Date: 11 September 2019
Accepted Date: 14 October 2019

Fund Project: Supported by the National Natural Science Foundation of China(No.51462010)the National Natural Science Foundation of China 51462010

Figures(8)

Silica coated bismuth-based yellow pigments with better acid resistance and temperature stability were successfully prepared by hydrolysis method using Bi_0.82V_0.45Mo_0.55O₄ and Na_0.5Bi_0.5(MoO₄) prepared by precipitation method. The as-obtained pigments were characterized by X-ray diffraction(XRD), transmission electron microscopy(TEM), X-ray fluorescence spectrometer(XRF) and Fourier transform infrared spectroscopy(FT-IR). The results showed that compact and uniform amorphous SiO₂·xH₂O coating layers with the thickness of around 100 nm were obtained under the volume ratio of H₂O to TEOS was 18, the ratio of n(Si)/n(Bi) was 4, T_b was 45℃, and v_d ≤ 0.3 mL/min. The coated pigments showed the nature of bright yellow, and the values of L^*, a^* and b^* were 78.85, -6.85 and 71.63, respectively. Compared with the uncoated pigments, the acid mass loss of coated pigments under the most optimized condition, after half an hour immersion in 1 mol/L hydrochloric acid, declined from 100% to 28.25% and the tolerable temperature was improved from 600℃ to 860℃.
- molybdenum bismuth vanadate,
- yellow pigment,
- SiO₂,
- coated pigment,
- stability
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