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Citation: JIANG Limei, ZOU Xiangyu, WEI Qinlei, SONG Qiong, DENG Shuang, ZHANG Hongbo, SU Chunhui. Preparation and Properties of Fluorine Containing CaO-P₂O₅-SiO₂-Na₂O-B₂O₃ Glass-ceramics[J]. Chinese Journal of Applied Chemistry, ;2015, 32(4): 442-446. doi: 10.11944/j.issn.1000-0518.2015.04.140235 shu

Preparation and Properties of Fluorine Containing CaO-P₂O₅-SiO₂-Na₂O-B₂O₃ Glass-ceramics

JIANG Limei ^a ,
ZOU Xiangyu ^a ,
WEI Qinlei ^a ,
SONG Qiong ^a,c ,
DENG Shuang ^a ,
ZHANG Hongbo ^a,, ,
SU Chunhui ^a,b

1.
a School of Chemistry Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, China;
2.
b Changchun Normal University Faculty of Chemistry, Changchun, 130032, China;
3.
c Jilin Teachers Institute of Engineering and Technology, Changchun 130032, China

Corresponding author: ZHANG Hongbo,
Received Date: 3 July 2014
Available Online: 24 December 2014
Fund Project: 国家"863"项目(2011AA030204) (2011AA030204)吉林省科技厅重点研究项目(20120341) (20120341)

By partially substituting of CaO with CaF₂,in CaO-P₂O₅-SiO₂-Na₂O-B₂O₃glass-ceramic system a new precursor powder was prepared by the sol-gel method. Its crystallization temperature was determined by TG-DSC at 865℃. The main crystal phase of the glass-ceramics is Na₆Ca₃Si₆O₁₈. The microstructures and properties of this glass-ceramics were characterized by X-ray diffractometry(XRD),Fourier transform infrared spectroscopy(FTIR),scanning electron microscopy(SEM) and in vitro assays. By addition of CaF₂,the volume density,bending strength and microhardness of the glass-ceramics are significantly improved,but the bioiogical activity of the glass-ceramics is maintained.
- sol-gel method,
- CaF₂,
- glass-ceramics,
- biological activity
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Preparation and Properties of Fluorine Containing CaO-P₂O₅-SiO₂-Na₂O-B₂O₃ Glass-ceramics