Citation: ZHANG Lei, ZHANG Ai-Qin, WANG Man, SHEN Gang-Yi. Capillary Electrophoresis Fingerprint of Arnebia Euchroma (Royle) Johnst[J]. Chinese Journal of Analytical Chemistry, ;2017, 45(11): 1727-1733. doi: 10.11895/j.issn.0253-3820.171120 shu

Capillary Electrophoresis Fingerprint of Arnebia Euchroma (Royle) Johnst

1.
Institute of Chinese Minority Traditional Medicine, The Key Laboratory of Chinese Minority Traditional Medicine(Ministry of Education of China), Minzu University of China, Beijing, 100081;
2.
College of Life and Environmental Science, Beijing Engineering Resaerch Center of Food Environment and Public Health Minzu University of China, Beijing, 100081

Received Date: 22 July 2017
Revised Date: 29 August 2017

Fund Project: This work was supported by the National Natural Science Foundation of China (Nos. 81573834, 81001595), the National Science and Technology Support Program, China (No. 2014BAC15B04) and Minzu University of China of the World First-class University and the First-class Discipline (No. YLDX01013).

A method of capillary electrophoresis fingerprint was developed for evaluation of the quality of Arnebia euchroma (Royle) Johnst. The samples were separated on a 50 μm×40 cm uncoated capillary separation column at separation voltage of 25 kV with 100 mmol/L borate buffer (pH 8.0) containing 25 mmol/L SDS and 20% (V/V) dehydrated alcohol as running buffer. The injection volume of sample was 0.5 psi×5 s and the detection wavelength was 214 nm. The results indicated that the samples of Arnebia euchroma (Royle) Johnst were well separated and detected in 35 min. With Shikonin peak as reference peak, 6 characteristic peaks of standard Arnebia euchroma (Royle) Johnst were determined. The quality discriminant analyses were accomplished for different kinds of samples named Arnebia euchroma (Royle) Johnst that purchased from eight sources by means of characteristic fingerprint peak analysis, similarity evaluation and cluster analysis. This method had good reproducibility, and could be used for the quality control of Arnebia euchroma (Royle) Johnst.
- Fingerprint,
- Arnebia euchroma (Royle) Johnst,
- Capillary electrophoresis,
- Quality control
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沈阳化工大学材料科学与工程学院沈阳 110142