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Citation: LI Shan, CHEN Chi-Lai, ZHU De-Quan, GUAN Ke, RUAN Zhi-Ming, LIU You-Jiang, YU Jian-Wen, XU Qing. Direct and Rapid Determination of Ammonia in Water Samples Using Ultraviolet Photoionization High Field-Asymmetric Waveform Ion Mobility Spectrometry[J]. Chinese Journal of Analytical Chemistry, ;2016, 44(11): 1679-1685. doi: 10.11895/j.issn.0253-3820.160469 shu

Direct and Rapid Determination of Ammonia in Water Samples Using Ultraviolet Photoionization High Field-Asymmetric Waveform Ion Mobility Spectrometry

LI Shan ^1,2, ,
CHEN Chi-Lai ¹ ,
ZHU De-Quan ² ,
GUAN Ke ¹ ,
RUAN Zhi-Ming ¹ ,
LIU You-Jiang ¹ ,
YU Jian-Wen ¹ ,
XU Qing ¹

1.
State Key Laboratory of Transducer Technology, Institute of Intelligent Machines, Chinese Academy Science, Hefei 230031, China;
2.
School of Engineering, Agricultural University, Hefei 230030

Received Date: 17 June 2016
Revised Date: 9 August 2016

Fund Project: This work was supported by the National Natural Science Foundation of China (No.61374016)

A novel on-site rapid detection method for ammonia detection in water was developed by using ultraviolet photoionization high field-asymmetric waveform ion mobility spectrometry (UV-FAIMS). The position of ammonia characteristic ion peak was acquired by the comparison between the characteristic compensation voltage (CV) in standard ammonia sample and trace amount ammonia in water. The relation between the positions of ammonia characteristic ion peaks under different dispersion voltages (DV) was studied. The values of α₂, α₄ were 2.21×10^-5 Td^-2 and -1.45323×10^-9 Td^-4, respectively. The different concentrations of ammonia in water was measured with a limit of detection (LOD) of 9.2 μg/L (S/N=3). This study provided a rapid, non-pretreatment means for the detection of ammonia in water matrices.
- Ammonia,
- Ultraviolet photoionization high field-asymmetric waveform ion mobility spectrometry,
- Water pollutants,
- On-site detection
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