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Citation: LI Jun-Jie, LIU Han-Bin, ZHANG Jia, HAN Juan, JIN Gui-Shan, ZHANG Jian-Feng. Determination of Dissolved Xe Concentration and Isotope Composition in Water by Mass Spectrometry[J]. Chinese Journal of Analytical Chemistry, ;2016, 44(11): 1748-1754. doi: 10.11895/j.issn.0253-3820.160255 shu

Determination of Dissolved Xe Concentration and Isotope Composition in Water by Mass Spectrometry

Beijing Research Institute of Uranium Geology, Beijing 100029, China

Received Date: 4 April 2016
Revised Date: 9 August 2016

A method was established to analyze the dissolved Xe concentration and Xe isotopes in water precisely with the self-design device of Xe extraction and separation line in combining with the Helix SFT noble gas mass spectrometer. The leak test and the background determination of the whole system proved the system was reliable. The large amount of Argon from Xe could be effectively removed by cycling temperature rising and falling method, which resulted in the elimination of the interference to the analysis of Xe concentration and isotopes. The limit of detection of the method for Xe concentration could reach as low as 10^-13-10^-14 L/L. The method was used for the measurement of the dissolved Xe in air saturated water (ASW), and the RSDs of Xe concentration, ¹²⁹Xe/¹³¹Xe and ¹³²Xe/¹³⁴Xe were 1.0%, 0.10% and 0.20% respectively, while the errors were 0.93%, 0.16% and 0.50% respectively.
- Water sample,
- Xenon isotopes,
- Extraction,
- Mass spectrometry
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