Citation: XIE Xiu-Man, SUN Wan-Yang, HUANG Jing-Yi, Navaneethakrishnan Polachi, TONG Ling, SUN Guo-Xiang. Preparative-High Performance Liquid Chromatography-based Multi-Dimensional Chromatography and Its Application in Traditional Chinese Medicine Research[J]. Chinese Journal of Analytical Chemistry, ;2016, 44(7): 1140-1147. doi: 10.11895/j.issn.0253-3820.160004
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Separation of the active ingredients of Chinese medicine is always difficult due to its complexity matrix. Recent years, the preparative-high performance liquid chromatography (Pre-HPLC)-based multidimensional chromatography combined with the characteristics of different separation technology improved the separation capability and efficiency, and was applied to the separation and purification of complex traditional Chinese medicine (TCM). In this review, the based principle, separation mode and key technology of preparative-HPLC-based multidimensional chromatography, as well as its application in TCM research were introduced.
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[4]
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[5]
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[6]
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[7]
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[8]
-
[9]
-
[10]
-
[11]
-
[12]
-
[13]
-
[14]
-
[15]
-
[16]
-
[17]
-
[18]
-
[19]
-
[20]
-
[21]
-
[22]
-
[23]
-
[24]
-
[25]
-
[26]
-
[27]
-
[28]
-
[29]
-
[30]
-
[31]
-
[32]
-
[33]
-
[34]
-
[35]
-
[36]
-
[37]
-
[38]
-
[39]
-
[40]
-
[41]
-
[42]
-
[43]
-
[44]
-
[45]
-
[46]
-
[47]
-
[48]
-
[49]
-
[50]
-
[51]
-
[52]
-
[53]
-
[54]
-
[55]
-
[56]
-
[57]
-
[58]
-
[59]
-
[60]
-
[61]
-
[62]
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