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Citation: Dan SHI, Zhang‐Lü HUANG, Su‐Ding YAN, Juan WANG, Guo‐Hong WANG. Preparation of Bi3TaO7/MXene Nanosheets Heterojunction for Photocatalytic Degradation of Sodium Sulfadiazine[J]. Chinese Journal of Inorganic Chemistry, ;2022, 38(8): 1487-1498. doi: 10.11862/CJIC.2022.166 shu

Preparation of Bi3TaO7/MXene Nanosheets Heterojunction for Photocatalytic Degradation of Sodium Sulfadiazine

  • Hubei Key Laboratory of Pollutant Analysis and Reuse Technology, School of Chemistry and Chemical Engineering, Hubei Normal University, Huangshi, Hubei 435002, China

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  • In this work, the Bi3TaO7/Ti3C2 composite photocatalysts were in-situ deposited on the surface of 2D Ti3C2 by electrostatic adsorption and solvothermal treatment using bismuth nitrate pentahydrate and tantalum pentachloride as the Bi and Ta sources, respectively. The effects of 2D Ti3C2 nanosheets on the microstructure of Bi3TaO7/ Ti3C2 were investigated by various physicochemical characterizations. The photocatalytic properties of as‐prepared samples were evaluated by visible light degradation of sodium sulfadiazine (SD‐Na) aqueous solution. The experimental results showed that the photocatalytic performance of the Bi3TaO7/Ti3C2 composites was significantly enhanced. Under the optimal conditions (the mass ratio of Ti3C2 to Bi3TaO7 was 0.02), the obtained BT2 sample exhibited the highest photocatalytic activity for degrading the SD‐Na aqueous solution and the apparent rate constant k value was 2.8 times higher than that of the pure Bi3TaO7 sample. The significant improvement of the Bi3TaO7/ Ti3C2 composite is attributed to the formation of heterojunction structure on the interface between Ti3C2 and Bi3TaO7, resulting in the rapid transfer and separation of photogenerated carriers.
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