Application of Polyoxometalates-Based Photosensitizers in Dye-Sensitized Solar Cells
- Corresponding author: LIU Li, liul515@nenu.edu.cn CHEN Wei-Lin, chenwl@nenu.edu.cn WANG En-Bo, wangeb889@nenu.edu.cn
Citation: GU Yi-Tong, CHEN Li, LI Jian-Ping, LIU Li, CHEN Wei-Lin, LIU Ding, WANG En-Bo. Application of Polyoxometalates-Based Photosensitizers in Dye-Sensitized Solar Cells[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(11): 1905-1920. doi: 10.11862/CJIC.2019.227
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(a) No titanium dioxide, (b) cTiO2=0.25 g·L-1
Electrolyte composition is as follows: 1.0 mol·L-1 1, 3-dimethylimidazolium iodide (DMII), 50 mmol·L-1 LiI, 30 mmol·L-1 I2, 0.5 mol·L-1 tert-butylpyridine and 0.1 mol·L-1 GNCS in the mixed solvent of acetonitrile and valeronitrile (85:15, V/V); Devices A and B were made with the electrolyte, employing the C101 and C102 sensitizers, respectively
Reagents and conditions: (ⅰ) metalic Na, anhydrous FeCl3, diethylsuccinate/tert-AmOH; (ⅱ) 2-ethylhexyl bromide, NMP/K2CO3 for DPP2a; DMAP/THF for DPP2b; (ⅲ) (1H-indole-5-yl)boronic acid, 2mol·L-1 K2CO3, Pd(PPh3)4, toluene, 65 ℃; (ⅳ) 1-Boc-indole-2-boronic acid, 2 mol·L-1 K2CO3, Pd(PPh3)4, toluene, 65 ℃
Amount of T was 0.00 g, 0.05g, 0.10 g, 0.20 g and 0.30 g, respectively, corresponding to T0@TiO2, T1@TiO2, T2@TiO2, T3@TiO2 and T4@TiO2